The following standards/reagents were purchased from Sigma Aldrich at 99 % purity: Anisole and the fluorinated benzenes fluorobenzene (FB), 1,2-difluorobenzene (12DFB), 1,3-difluorobenzene (13DFB), 1,4-difluorobenzene (14DFB), 1,2,3-trifluorobenzene (123TFB), 1,2,4-trifluorobenzene (124TFB), 1,3,5-trifluorobenzene (135TFB), 1,2,3,4-tetrafluoro-benzene (1234TFB), 1,2,3,5-tetrafluoro-benzene (1235TFB), 1,2,4,5-tetrafluorobenzene (1245TFB), pentafluorobenzene (PFB) and hexafluorobenzene (HFB). Also, the solvents hexane, acetonitrile and isopropyl alcohol and the proteins l -tyrosine (l -Tyr), phenylalanine (Phe) and pentafluorophenylalanine (F5Phe) are purchased from Sigma Aldrich. Deionized water was obtained from a Millipore Q-POD water deionizer and purifier.
Trifluorobenzene
Manufactured by Merck Group
trifluorobenzene is a colorless, volatile organic compound used in laboratory settings. It has the chemical formula C6H3F3 and is a member of the aromatic fluorinated benzene family. The main function of trifluorobenzene is as a solvent and reagent in chemical research and analysis.
Automatically generated - may contain errors
Lab products found in correlation
Pentafluorobenzene, by Merck Group (3 mentions)
Fluorobenzene, by Merck Group (2 mentions)
Anisole, by Merck Group (2 mentions)
1 2 difluorobenzene, by Merck Group (2 mentions)
1 3 difluorobenzene, by Merck Group (2 mentions)
1 4 difluorobenzene, by Merck Group (2 mentions)
Pentafluorophenylalanine f5phe, by Merck Group (2 mentions)
Q pod, by Merck Group (2 mentions)
Hexane, by Merck Group (2 mentions)
Acetonitrile, by Merck Group (2 mentions)
Isopropyl alcohol, by Merck Group (2 mentions)
Diethyl malonate, by Merck Group (1 mentions)
Trimethylsilyl cyanide, by Merck Group (1 mentions)
Triethoxysilane, by Merck Group (1 mentions)
Avance dpx 300 mhz nmr spectrometer, by Bruker (1 mentions)
Tert butyl alcohol, by Merck Group (1 mentions)
3 protocols using trifluorobenzene
1
Fluorinated Benzene Compounds Evaluation
2
Fluorinated Benzene Compounds Evaluation
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The following standards/reagents were purchased from Sigma Aldrich at 99 % purity: Anisole and the fluorinated benzenes fluorobenzene (FB), 1,2-difluorobenzene (12DFB), 1,3-difluorobenzene (13DFB), 1,4-difluorobenzene (14DFB), 1,2,3-trifluorobenzene (123TFB), 1,2,4-trifluorobenzene (124TFB), 1,3,5-trifluorobenzene (135TFB), 1,2,3,4-tetrafluoro-benzene (1234TFB), 1,2,3,5-tetrafluoro-benzene (1235TFB), 1,2,4,5-tetrafluorobenzene (1245TFB), pentafluorobenzene (PFB) and hexafluorobenzene (HFB). Also, the solvents hexane, acetonitrile and isopropyl alcohol and the proteins l -tyrosine (l -Tyr), phenylalanine (Phe) and pentafluorophenylalanine (F5Phe) are purchased from Sigma Aldrich. Deionized water was obtained from a Millipore Q-POD water deionizer and purifier.
3
Synthesis of Fluorinated Benzene Derivatives
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Unless stated
otherwise, all
reactions were carried out in air. Solvents were distilled and dried
as required. Pentafluorobenzene, 1,2,4,5-tetrafluorobenzene, 1,3,5-trifluorobenzene,
sodium tert-butoxide, diethyl malonate, trimethylsilyl
cyanide, triethoxysilane, triflimide, tert-butyl
alcohol, tBuNC, KCN, and norbornene were
purchased from Sigma-Aldrich and used as received. (AdCAAC)AuCl6c and Me2CAAC47 were obtained according to a literature procedure. 1H, 13C{1H}, and 19F NMR spectra were recorded
using a Bruker Avance DPX-300 MHz NMR spectrometer. 1H
NMR spectra (300.13 MHz) and 13C{1H} (75.47
MHz) were referenced to CD2Cl2 at δ 5.32
(13C, δ 54.0), C6D6 at δ
7.16 (13C, δ 128.4), CDCl3 at δ
7.26 (δ 13C 77.2), or C6D5Br
at δ 7.30 for the most downfield signal (13C, δ
122.5 for the most upfield signal) ppm. 19F NMR spectra
(282.4 MHz) were referenced externally to CFCl3 and internally
to C6F6 (δF −164.9).
IR spectra were recorded using a PerkinElmer Spectrum One FT-IR spectrometer
equipped with a diamond ATR attachment. Elemental analyses were performed
by the London Metropolitan University.
otherwise, all
reactions were carried out in air. Solvents were distilled and dried
as required. Pentafluorobenzene, 1,2,4,5-tetrafluorobenzene, 1,3,5-trifluorobenzene,
sodium tert-butoxide, diethyl malonate, trimethylsilyl
cyanide, triethoxysilane, triflimide, tert-butyl
alcohol, tBuNC, KCN, and norbornene were
purchased from Sigma-Aldrich and used as received. (AdCAAC)AuCl6c and Me2CAAC47 were obtained according to a literature procedure. 1H, 13C{1H}, and 19F NMR spectra were recorded
using a Bruker Avance DPX-300 MHz NMR spectrometer. 1H
NMR spectra (300.13 MHz) and 13C{1H} (75.47
MHz) were referenced to CD2Cl2 at δ 5.32
(13C, δ 54.0), C6D6 at δ
7.16 (13C, δ 128.4), CDCl3 at δ
7.26 (δ 13C 77.2), or C6D5Br
at δ 7.30 for the most downfield signal (13C, δ
122.5 for the most upfield signal) ppm. 19F NMR spectra
(282.4 MHz) were referenced externally to CFCl3 and internally
to C6F6 (δF −164.9).
IR spectra were recorded using a PerkinElmer Spectrum One FT-IR spectrometer
equipped with a diamond ATR attachment. Elemental analyses were performed
by the London Metropolitan University.
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