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S4800 field emission scanning electron microscope

Manufactured by Bruker
Sourced in Japan, United States

The S4800 is a field emission scanning electron microscope (FESEM) manufactured by Bruker. It is designed to provide high-resolution imaging and analysis of a wide range of materials and samples. The S4800 utilizes a field emission electron source to generate a focused electron beam, allowing for high-resolution imaging at low accelerating voltages. The microscope is equipped with various detectors and analytical capabilities to facilitate comprehensive characterization of samples.

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4 protocols using s4800 field emission scanning electron microscope

1

SEM Analysis of Welding Particles

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Welding samples were dispersed onto 47-mm Nuclepore polycarbonate filters (Whatman, Clinton, PA). The filters were mounted onto aluminum stubs with silver paste. The welding particles were viewed using a Hitachi S4800 field emission scanning electron microscope (Bruker, Madison, WI).
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2

Comprehensive Characterization of Perovskite Solar Cells

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The current density-voltage (J-V) characterization of PSCs was carried out using a Keithley 2400 source meter under a simulated AM 1.5 illumination (100 mW cm−2, NewPort, 94043 A SOLAR SIM) at a scan rate of 200 mV s−1. The incident-photon-to-current efficiency (IPCE) measurement was performed through an Enlitech QE-R Quantum Efficiency Measurement System (QE-R3018). The crystal structures of the MAPbI3 films were characterized by using a Bruker D8 ADVANCE X-ray diffraction (XRD) equipment. The morphology of the MAPbI3 layer was obtained using a Hitachi S-4800 field emission scanning electron microscope (SEM) and a Bruker atomic force microscope (AFM). Energy dispersive spectroscopy (EDS) was conducted by using an EDS device connected to SEM. The thicknesses of the NiOx, MAPbI3 and PC61BM films were determined using a Bruker DektakXT Stylus Profiler. The photoluminescence (PL) and time-resolved PL (TRPL) spectra were measured by using an Edinburgh FLS980 fluorescence spectrophotometer with an excitation at 550 nm. The impedance characteristics of the devices were measured via a Wayne Kerr 6500B analyzer.
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3

Characterization of Perovskite Solar Cells

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The current density–voltage (J–V) characterization of PSC was carried out using a Keithley 2400 source meter under a simulated AM 1.5 illumination (100 mW·cm−2, NewPort, 94043A SOLAR SIM, Irvine, CA, USA) at a scan rate of 200 mV·s−1. The incident-photon-to-current efficiency (IPCE) measurement was performed through an Enlitech QE-R Quantum Efficiency Measurement System (QE-R3018, Taiwan, China). The crystal structures of the MAPbI3 films were characterized by using a Bruker D8 ADVANCE X-ray diffraction (XRD) device (Karlsruhe, Germany). The morphology of the MAPbI3 layer was obtained using a Hitachi S-4800 field emission scanning electron microscope (SEM, Tokyo, Japan) and a Bruker atomic force microscope (AFM). The thicknesses of the NiOx, MAPbI3 and PC61BM films were determined using a Bruker DektakXT Stylus Profiler. The photoluminescence (PL) spectra were measured using an Edinburgh FLS980 fluorescence spectrophotometer (Livingston, UK) with an excitation at 550 nm. The impedance characteristics of the devices were measured via a Wayne Kerr 6500B analyzer (London, UK).
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4

Scanning Electron Microscopy of Welding Fume

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Spot welding fume was collected onto 47-mm Nuclepore polycarbonate filters (Whatman, Clinton, PA, USA). The filters were mounted onto aluminum stubs with silver paste. The collected welding particles were viewed using a Hitachi S4800 field emission scanning electron microscope (Bruker, Madison, WI, USA).
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