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2400 chns elemental analyzer

Manufactured by PerkinElmer
Sourced in United States

The 2400 CHNS elemental analyzer is a laboratory instrument designed to determine the carbon, hydrogen, nitrogen, and sulfur content in organic and inorganic samples. It utilizes combustion and gas chromatography techniques to accurately measure the elemental composition of a wide range of materials.

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3 protocols using 2400 chns elemental analyzer

1

Characterization of Organic Compounds

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The 1H and 13C spectra were recorded in DMSO or D2O solutions in 5 mm tubes, at room temperature, with a Bruker spectrometer (Karlsruhe, Germany) at 500 (1H) and 125 (13C) MHz, with the deuterium signal of the solvent as the lock and TMS as internal standard.
Melting points were determined on a Hinotek X-4 melting point apparatus (Ningbo, China). Elemental analyses were performed with a Perkin-Elmer 2400 CHNS elemental analyzer (Waltham, MA, USA). Merck Kieselgel 60F254 plates (Budapest, Hungary) were used for TLC. The microwave reactions were performed with a CEM Discover SP microwave reactor (Matthwes, NC, USA).
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2

Synthesis and Spectroscopic Characterization of Cyclic Imines

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Melting points were determined on a Hinotek X-4 (Hinotek Technology Co., Ltd., Ningbo, China) melting point apparatus. Elemental analyses were performed with a Perkin-Elmer 2400 CHNS elemental analyzer (Perkin-Elmer, Waltham, MA, USA) in the Institute of Pharmaceutical Chemistry, University of Szeged. Merck Kieselgel 60F254 plates (Merck Hungary, Budapest, Hungary) were used for the TLC. The microwave reactions were performed with a CEM Discover SP microwave reactor (CEM, Matthwes, NC, USA).
The starting cyclic imines 3,4-dihydroisoquinoline (2) [18 (link)]; 3,4-dihydro-β-carboline (4) [19 (link)]; 6,7-dihydrothieno[3,2-c]pyridine (5) [20 (link)]; and 4,5-dihydro-3H-benz[c]azepine (6) [21 (link),22 (link)] were synthesized according to the literature.
The 1H-and 13C-NMR spectra were recorded in CDCl3 or [D6]DMSO solution in 5 mm tubes at room temperature, on a Bruker Avance II spectrometer (Bruker, Karlsruhe, Germany) at 500 (1H) and 125 (13C) MHz, with the deuterium signal of the solvent as the lock and TMS as the internal standard. All spectra (1H, 13C) were acquired and processed with the standard BRUKER software.
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3

Spatial Energy Potential of Cassava Rhizomes

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Quantitative data analysis (quantity) of cassava rhizomes for the study of spatial energy potential: -Biomass Yield Ratio Crop Residue Ratios: (CRR) is the amount of biomass for energy generation without residue.
-Energy potential of biomass (kiloton per oil equivalent; toe). -Details on area, quantity of existing biomass raw materials, and the estimation of potential to commerce acquisition for biomass feedstock.
-Data analysis on the quality of cassava rhizomes: -Physical properties of biomass fuel such as: size, size distribution, moisture content, and appearance density.
-Proximate analysis of biomass fuel such as: moisture, ash, volatile matter, and fixed carbon. Analysis was performed according to ASTM E 1617-94 [12] and ASTM E 1755-01 [13] , while according to ASTM D 2015 [14] , a bomb calorimeter was adopted for different heating values.
-The ultimate analysis of biomass fuels such as: C, H, N, S, and O was conducted, moreover, elemental analyses of carbon (C), hydrogen (H), and nitrogen (N) were done with the use of a PerkinElmer 2400 CHNS Elemental Analyzer. The sulfur (S) content was determined by the use of a plasma spectrometry, while that of optical analysis was carried with a Sector ICP-OES spectrometer as established by titration according to [15] .
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