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Butyl 3 mercaptopropionate

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Butyl 3-mercaptopropionate is a chemical compound used as a laboratory reagent. It is a clear, colorless liquid with a characteristic odor. The compound is often used in various chemical synthesis and analysis procedures.

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Lab products found in correlation

1 hexanethiol, by Merck Group (2 mentions) Triethylamine, by Merck Group (2 mentions) Butyl acrylate, by Merck Group (2 mentions) Divinyl sulfone, by Merck Group (1 mentions) 2 2 6 6 tetramethyl 1 piperidinyloxy free radical, by Merck Group (1 mentions) 2 2 6 6 tetramethylpiperidin 1 yl oxyl, by Merck Group (1 mentions) 2 2 6 6 tetramethylpiperidine, by Merck Group (1 mentions) Diethyl fumarate, by Merck Group (1 mentions) Diethyl maleate, by Merck Group (1 mentions) N propyl maleimide, by Merck Group (1 mentions) 4 hexen 3 one, by Merck Group (1 mentions) Camphorquinone, by Merck Group (1 mentions) Benzophenone, by Merck Group (1 mentions) Ethyl 4 dimethylaminobenzoate, by Merck Group (1 mentions) Trimethylolpropane triacrylate, by Merck Group (1 mentions)

3 protocols using butyl 3 mercaptopropionate

1

Synthesis of Thiol-Ene Photocurable Resins

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2,2,6,6-Tetramethyl piperidine (TMP), divinyl sulfone (DVS), 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical (TEMPO), 1-hexanethiol (HT), butyl 3-mercaptopropionate (BT), butyl acrylate, triethylamine (TEA), (2,2,6,6-Tetramethylpiperidin-1-yl) oxyl (TEMPO), and diethyleneglycol diethyl ether (DEGDE), triethylene glycol diacrylate (TEGDA) were purchased from Sigma-Aldrich. Pentaerythritol tetra(3-mercaptopropionate) (PETMP) was donated by Bruno Bock. All chemicals were used as received. Tetra (2-mercaptoethyl) silane (SiTSH) was synthesized according to a previously reported procedure.37 Molecular structures are depicted in Fig. 1.
Zhang X., Huang S., Podgórski M., Han X., Claudino M, & Bowman C.N. (2018). Assessment of TEMPO as a Thermally Activatable Base Generator and Its Use in Initiation of Thermally-Triggered Thiol–Michael Addition Polymerizations. Polymer chemistry, 9(32), 4294-4302.
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2

Radical Polymerization of Functional Monomers

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Butyl 3-mercaptopropionate (BMP), 1-hexanethiol (HT), ethyl vinyl sulfone (EVS), 1-butyl acrylate (BA), N-propylmaleimide (PMI), diethyl maleate (DEM), diethyl fumarate (DEF), 4-hexen-3-one (HEO), and ethylene glycol diethyl ether (EGDE) were purchased from Sigma-Aldrich. All monomers were used as received. The photobase generator (PBG) NPPOC-TMG and hexyl vinyl sulfonate (HVS) were synthesized according to previous literature42 .
Huang S., Kim K., Musgrave G.M., Sharp M., Sinha J., Stansbury J.W., Musgrave C.B, & Bowman C.N. (2021). Determining Michael Acceptor Reactivity from Kinetic, Mechanistic, and Computational Analysis for the Base-catalyzed Thiol-Michael Reaction. Polymer chemistry, 12(25), 3619-3628.
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3

Photopolymerization of PETMP-Based Resins

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Pentaerythritol tetra(3-mercaptopropionate) (PETMP) was purchased from Bruno Bock. Trimethylolpropane triacrylate (TMPTA), benzophenone (BP), triallyl-1,3,5-triazine-2,4,6-(1H,3H,5H)-trione (TTT), tricyclo[5.2.1.02,6]decanedimethanol diacrylate (TCDDA), 2-hydroxy-1-[4-(2-hydroxyethoxy)phenyl]-2-methyl-1-propanone (Irgacure 2959), camphorquinone (CQ), triethylamine (TEA), ethyl 4-(dimethylamino)benzoate (EDAB), isopropyl-thioxanthone (ITX), butyl 3-mercaptopropionate, and butyl acrylate were purchased from Sigma-Aldrich without further purification.
Zhang X., Xi W., Huang S., Long K, & Bowman C.N. (2017). Wavelength-Selective Sequential Polymer Network Formation Controlled with a Two-Color Responsive Initiation System. Macromolecules, 50(15), 5652-5660.
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