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Drx nmr spectrometer

Manufactured by Bruker
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The DRX NMR spectrometer is a nuclear magnetic resonance (NMR) instrument designed for analytical and research applications. It is capable of detecting and analyzing the magnetic properties of atomic nuclei within a sample, providing information about the chemical structure and composition of the material.

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Lab products found in correlation

Jem 2100, by JEOL (3 mentions) 90 plus, by Brookhaven Instruments (2 mentions) F 4600, by Hitachi (2 mentions) 90 plus particle size analyzer, by Brookhaven Instruments (2 mentions) Jem 2100 equipment, by JEOL (2 mentions) Uv 3600, by Hitachi (1 mentions) Uv 3600 uv vis nir, by Shimadzu (1 mentions) F 4600 spectrometer, by Hitachi (1 mentions) Ivis lumina k, by PerkinElmer (1 mentions) Nicolet is5 ftir spectrometer, by Thermo Fisher Scientific (1 mentions) Liquid helium quartz cryostat, by Oxford Instruments (1 mentions) Emx spectrometer, by Oxford Instruments (1 mentions) Er041xg microwave bridge, by Oxford Instruments (1 mentions) Cary 50 spectrometer, by Agilent Technologies (1 mentions) Er4116dm, by Oxford Instruments (1 mentions) Ethyl ether, by Merck Group (1 mentions) Tetrahydrofuran thf, by Merck Group (1 mentions) Dimethylformamide dmf, by Merck Group (1 mentions) Uv 3600, by Shimadzu (1 mentions) Uv 3600 spectrophotometer, by Shimadzu (1 mentions)

Close spelling variants of this product

Avance DRX 500 MHz NMR spectrometer Avance DRX 500 NMR spectrometer DRX 400 MHz NMR spectrometer DRX-600 NMR spectrometer DRX-400 NMR spectrometer DRX-500 NMR spectrometer Avance DRX NMR spectrometer AVVANCE DRX-400 NMR spectrometer DRX-600 MHz NMR spectrometer 1H-NMR 400 DRX Spectrometer

6 protocols using drx nmr spectrometer

1

Detailed Characterization of DPPA Nanoparticles

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1H NMR and 13C NMR spectra were performed on a Bruker DRX NMR spectrometer in CDCl3 (δ = 7.26 ppm) at 298 K as the internal standard. UV-vis and fluorescence spectra were measured on a Shimadzu spectrophotometer, from Japan, (UV-3600) and a HITACHI spectrometer (F-4600, Japan), respectively. TEM of the nanoparticles were measured on equipment (JEOL JEM-2100). Dynamic light scattering (DLS) of DPPA NPs was tested on a particle size analyzer (90 Plus, Brookhaven Instruments, United States). Fluorescence imaging of DPPA NPs in nude mice was recorded on an IVIS spectrum.
Shen J., Pan L., Zhang X., Zou Z., Wei B., Chen Y., Tang X, & Zou D. (2022). Delivering Singlet Oxygen in Dark Condition With an Anthracene-Functionalized Semiconducting Compound for Enhanced Phototheranostics. Frontiers in Bioengineering and Biotechnology, 10, 781766.
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2

Multimodal Characterization of Nanoparticles

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All chemicals were purchased from Sigma and used without further purification. The 1H NMR and 13C NMR spectra were recorded on a Bruker DRX NMR spectrometer (500 MHz) in CDCl3 solution at 298 K with a solvent residual as the internal standard (CDCl3, δ = 7.26 ppm). UV-vis spectra were measured on a spectrophotometer (UV-3600 UV-Vis-NIR, Shimadzu, Japan). The fluorescence spectra were recorded on an F4600 spectrometer (HITACHI, Japan). DLS was performed with a 90 Plus particle size analyzer (Brookhaven Instruments, USA). TEM of the nanoparticles was carried out using JEOL JEM-2100 equipment. The bio-images of the tumor, heart, liver, spleen, and kidney were recorded on a PerkinElmer IVIS Lumina K.
Zou J., Yin Z., Wang P., Chen D., Shao J., Zhang Q., Sun L., Huang W, & Dong X. (2018). Photosensitizer synergistic effects: D–A–D structured organic molecule with enhanced fluorescence and singlet oxygen quantum yield for photodynamic therapy †Electronic supplementary information (ESI) available. See DOI: 10.1039/c7sc04694d. Chemical Science, 9(8), 2188-2194.
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3

Spectroscopic Characterization of Organometallic Complexes

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All electronic absorption spectra were collected in a 1 cm quartz cuvette with a magnetic spin bar inside. Room temperature electronic absorption spectra for determining extinction coefficients were recorded on a Cary 50 spectrometer. Temperature controlled time dependent electronic absorption spectra were recorded either on a Cary 60 spectrometer equipped with Quantum Northwest TC1 temperature controller and stirrer, or on an 8453E Agilent UV-vis spectrometer equipped with an Unisoku Unispeks cryostat. Cyclic voltammetry was performed using a CHI600C electrochemical analyzer under Ar atmosphere with 0.1 M tetrabutylammonium hexafluorophosphate as the supporting electrolyte. A 2.0 mm glassy carbon electrode was used as working electrode; a Pt wire was used as counter electrode; a Ag wire was used as references electrode with ferrocenium/ferrocene(FeCp2+/0) couple as internal standard. All potentials are referenced to FeCp2+/0 couple. Solid-state IR spectra were collected on a Thermo Scientific Nicolet iS5 FT-IR spectrometer equipped with an iD5 ATR accessory. X-band EPR spectra were recorded as frozen solutions using a Bruker EMX spectrometer equipped with an ER041XG microwave bridge, an Oxford Instrument liquid-helium quartz cryostat, and a dual-mode cavity (ER4116DM). Magnetic moments were done by Evans's method at 298 K in CH2Cl2 on a Bruker DRX NMR spectrometer.41
Sun C., Oswald V.F., Hill E.A., Ziller J.W, & Borovik A.S. (2021). Investigation of Iron–Ammine and Amido Complexes within a C3-Symmetrical Phosphinic Amido Tripodal Ligand. Dalton transactions (Cambridge, England : 2003), 50(32), 11197-11205.
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4

Synthesis and Characterization of Photoresponsive Nanomaterials

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Poly(ethylene glycol)-amine (PEG-NH2), 2-(diisopropylamino)ethyl methacrylate (99 %), azobisisobutyrontrile (AIBN, 98 %), thiazolyl blue tetrazolium bromide (MTT, 97.5 %), 2-[2-[2-chloro-3-[[1,3-dihydro-1,1-dimethyl-3-(4-sulfobutyl)-2H-benzo[e]indol-2-ylidene]-ethylidene]-1-cyclohexen-1-yl]-ethenyl]-1,1-dimethyl-3-(4-sulfobutyl)-1H-benzo[e]indolium hydroxide inner salt (IR820, 80 %), O2-(2,4-dinitrophenyl) 1-[(4-ethoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate (JSK, 99 %), ethyl ether (99.9 %), dimethylformamide (DMF, 99.5 %) and tetrahydrofuran (THF) were purchased from Sigma-Aldrich. 1-(chloromethyl)-4-vinylbenzene, 4-cyano-4-(phenylcarbonothioylthio)pentanoic acid N-succinimidyl ester (CPPA) were purchased from Adamas and were used without further purification. The 1HNMR and 13CNMR spectra were measured on Bruker DRX NMR spectrometer at 298 K as the internal standard with solvent residual (400 MHz). UV–vis spectra were recorded on a UV-Vis-NIR spectrophotometer (Agilent, Carry 5000). Fluorescence spectra were measured on an FS500 spectrometer (Edinburgh, UK). Dynamic light scattering (DLS) was measured on a Litesizer 500 size analyzer. Transmission electron microscope (TEM) images were measured on equipment of JEOL JEM-2100.
Zou J., Li Z., Zhu Y., Tao Y., You Q., Cao F., Wu Q., Wu M., Cheng J., Zhu J, & Chen X. (2024). pH/GSH dual responsive nanosystem for nitric oxide generation enhanced type I photodynamic therapy. Bioactive Materials, 34, 414-421.
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5

Characterization of PDPP Nanoparticles

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1H NMR spectra were observed using a Bruker DRX NMR spectrometer in CDCl3 (δ = 7.26 ppm) at 298 K as the internal standard. UV-vis and fluorescence spectra were measured using a Shimadzu spectrophotometer from Japan (UV-3600) and a FS970 spectrometer (Japan), respectively. TEM of the nanoparticles was measured on equipment (JEOL JEM-2100). Dynamic light scattering (DLS) of PDPP NPs was tested using a particle size analyzer (90 Plus, Brookhaven Instruments, United States).
Cui C., Su X., Guo Y., Zhu J., Chen Z., Qin W., Guo Y, & Tao W. (2022). Enhancing electron transfer of a semiconducting polymer for type I photodynamic and photothermal synergistic therapy. Frontiers in Bioengineering and Biotechnology, 10, 1004921.
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6

Nanoparticle Characterization Protocol

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General chemicals were purchased from Sigma (Shanghai, Co. Ltd) and used without further purification. 1H NMR and 13C NMR spectra were measured on a Bruker DRX NMR spectrometer at 298 K in a CDCl3 solution with residual solvent as the internal standard. UV-vis spectra were measured on a UV-3600 spectrophotometer (Shimadzu, Japan). Fluorescence spectra were recorded on an F-4600 HITACHI spectrophotometer from Japan. DLS was carried out on a 90 Plus particle size analyzer (Brookhaven Instruments, USA). TEM of the nanoparticles was performed on JEOL JEM-2100 equipment. Fluorescence bioimaging of tumors and the main organs (heart, liver, spleen, lungs and kidneys) was performed on a PerkinElmer IVIS Lumina K.
Zou J., Wang P., Wang Y., Liu G., Zhang Y., Zhang Q., Shao J., Si W., Huang W, & Dong X. (2018). Penetration depth tunable BODIPY derivatives for pH triggered enhanced photothermal/photodynamic synergistic therapy †Electronic supplementary information (ESI) available. See DOI: 10.1039/c8sc02443j. Chemical Science, 10(1), 268-276.
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