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Ultrascan 1000 ccd tv camera

Manufactured by Ametek

The Ultrascan 1000 CCD TV camera is a laboratory equipment product manufactured by Ametek. It captures images using a charge-coupled device (CCD) sensor. The camera has a resolution of 1024 x 768 pixels and is capable of capturing video at a rate of 30 frames per second.

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2 protocols using ultrascan 1000 ccd tv camera

1

Experimental Electron Ronchigram Acquisition

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Electron Ronchigrams were acquired experimentally on a double corrected JEOL 3100R05 with a Gatan Ultrascan 1000 CCD TV camera. A typical alignment operating condition was used: 300 keV with a 150 μm objective aperture (110 mrad convergence angle), 8 cm camera length, and one second acquisition time. Ronchigrams were formed with 50 nm thick amorphous Silicon Nitride TEM grids (Norcada Inc.). Defocus and two-fold astigmatism were intentionally introduced using the JEOL COSMO software, and series of Ronchigrams with varying defocus were acquired with custom software. Acquired Ronchigrams were post-processed with practically the same procedure as the simulated Ronchigrams: images were cropped to the largest square inscribed by the objective aperture, down-sampled to 512x512 pixels, normalized to the maximum pixel value, and converted to 8-bit grayscale.
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2

Comprehensive Characterization of Mesoporous Silica Particles

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UV-Vis measurements are acquired by an 8453 UV-Vis Chem station spectrophotometer produced by Agilent Technologies. Zeta potential of mSPs was measured at 25C using a Zetasizer Nano ZS instrument (Malvern Instruments Ltd, Malvern, Worcestershire, UK). Circular Dichroism (CD) spectra were obtained by a JASCO J-815. TEM images obtained by utilizing JEOL 3011 high-resolution electron microscope equipped with a CCD camera and a field emission gun (FEG) operating at 300 kV. SEM images were obtained with FEI Helios 650 Nanolab SEM/FIB. STEM images obtained with JEOL 2100 Probe-Corrected Analytical electron microscope equipped with a Gatan Ultrascan 1000 CCD TV camera and a field emission gun (FEG) operating at 200KV. The Fourier transform infrared spectroscopy (FTIR, Thermo-Nicolet IS-50); energy dispersive X-ray spectrometry (EDS, FEI Helios 650 Nanolab SEM/FIB and JEOL 2100F) and X-ray photoelectron spectrometry (XPS, Kratos Analytical AXIS Ultra) and X-Ray diffractometer (XRD, Rigaku Rotating Anode with Cu Kα radiation generated at 40 kV and 100 mA) were used to exam the composition of particles. Fluorescence data is obtained by a Jobin Yvon Horiba FluoroMax-3 instrument.
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