Regarding the reagents used: cisplatin (cis-dichlorodiammine platinum (II), 99.9%), potassium tetrachloropalladate (II) (K2PdCl4, 98%), and the amine spermine (N,N′-bis(3-aminopropyl)-1,4-diaminobutane, 99%) were obtained from Sigma-Aldrich (Sintra, Portugal). All reagents were of analytical grade. Euthasol® solution (400 mg/mL pentobarbital sodium) was purchased from Le Vet (Oudewater, The Netherlands). The Pd2Spm complex was synthesized as described elsewhere [54 (link),55 (link)].
Potassium tetrachloropalladate 2 k2pdcl4
Manufactured by Merck Group
Sourced in Portugal
Potassium tetrachloropalladate (II) (K2PdCl4) is a chemical compound used as a laboratory reagent. It is a crystalline, yellow-orange solid that is soluble in water and other polar solvents. The compound contains palladium in the +2 oxidation state and is commonly used in various chemical reactions and analyses.
Automatically generated - may contain errors
Lab products found in correlation
Cisplatin cis dichlorodiammine platinum 2, by Merck Group (3 mentions)
Fetal bovine serum (fbs), by Thermo Fisher Scientific (3 mentions)
Spermine n n bis 3 aminopropyl 1 4 diaminobutane, by Merck Group (2 mentions)
Polyvinylpyrrolidone pvp, by Merck Group (1 mentions)
Ethanol, by Merck Group (1 mentions)
Ascorbic acid, by Merck Group (1 mentions)
Potassium chloride (kcl), by Merck Group (1 mentions)
Ethylene glycol, by Merck Group (1 mentions)
Nafion, by Merck Group (1 mentions)
Vulcan carbon xc 72r, by Cabot (1 mentions)
N butyllithium in hexane, by Merck Group (1 mentions)
Molybdenum 4 sulfide mos2 powder, by Merck Group (1 mentions)
Molybdenum 4 selenide mose2 powder, by Merck Group (1 mentions)
Tungsten 4 sulfide ws2 powder, by Merck Group (1 mentions)
Nafion perfluorinated resin solution, by Merck Group (1 mentions)
Acetonitrile, by Nanjing Chemical Reagent (1 mentions)
Pb no3 2, by Nanjing Chemical Reagent (1 mentions)
Rpmi 1640 cell culture medium, by Merck Group (1 mentions)
Tracecert, by Merck Group (1 mentions)
Arium pro water purification system, by Sartorius (1 mentions)
5 protocols using potassium tetrachloropalladate 2 k2pdcl4
1
Synthesis and Characterization of Pd(II)-Spermine Complex
2
Synthesis of PVP-Stabilized Pd Catalyst
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Polyvinylpyrrolidone (PVP, mol wt 40 000, Sigma-Aldrich), ethylene glycol (EG, 99.8%, Sigma), ascorbic acid (AA, 99.0%, Sigma-Aldrich), potassium tetrachloropalladate(ii) (K2PdCl4, 99%, Sigma-Aldrich), Vulcan carbon XC-72R (Cabot), ethanol (96%, industrial grade) for the dispersion of the carbon support, ethanol (99.7%, Sigma-Aldrich) as fuel, Nafion® (5 wt% in isopropanol, Sigma-Aldrich), potassium chloride (99.7%, Sigma-Aldrich) to saturated the reference electrode dissolution and potassium hydroxide (KOH 85%, Sigma-Aldrich) were used as received.
3
Synthesis of Transition Metal Dichalcogenides and Catalysts
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Molybdenum(IV) sulfide (MoS2) powder, molybdenum(IV) selenide (MoSe2) powder, tungsten(IV) sulfide (WS2) powder, n-butyllithium in hexane (2.5 M), rhodium(III) chloride (RhCl3), potassium tetrachloropalladate(II) (K2PdCl4), and Nafion perfluorinated resin solution (5 wt% in a mixture of low aliphatic alcohols and water, containing 45% water) were purchased from Sigma–Aldrich (St. Louis, MO); aluminum oxide powder (0.05 CR) was purchased from BAIKOWSKI (USA); NaBH4 and SnO were purchased from the First Reagent Factory (China); potassium tetrachloroplatinate(II) (K2PtCl4) and Pt/C (5 wt%) were purchased from Macklin (China); acetonitrile, polyvinylpyrrolidone (PVP), CuSO4, Pb(NO3)2, and Bi(NO3)3 were purchased from Nanjing Chemical Reagent (China); iodine and tungsten(IV) selenide (WSe2) powder were purchased from Aladdin Industrial Corporation (China). All aqueous solutions were prepared with Millipore water (18.2 MΩ cm resistivity).
4
Trace Metal Analysis of Biological Samples
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Polypropylene 10 mL tubes with high-density polyethylene screw caps (Ref# 62.9924.284) used for sample digestions were from Sarstedt (Nümbrecht, Germany). Nitric acid (HNO3, TraceSELECT™, ≥69.0%) and hydrochloric acid (HCl, TraceSELECT™, ≥30%) were purchased from Honeywell Fluka™ (Düsseldorf, Germany). For ICP-MS determinations, the multi-element standard solution TraceCERT® (100 mg/L), ICH Q3D oral, Standard 2 solution from Merck KGaA (Darmstadt, Germany) and the internal standard solution ICP-MS-200.8-IS-1 (100 mg/L of Sc, Y, In, Tb, Bi) from AccuStandard® (New Haven, CT, USA) were used. Ultrapure water (18.2 MΩ.cm at 25 °C) was obtained with an Arium® pro water purification system (Sartorius, Goettingen, Germany). Animals were euthanized with Euthasol® solution (400 mg/mL pentobarbital sodium) acquired from Le Vet (Oudewater, The Netherlands). Cisplatin (cis-dichlorodiammine platinum(II), 99.9%), potassium tetrachloropalladate (II) (K2PdCl4, 98%), spermine (N,N’-bis(3-aminopropyl)-1,4-diaminobutane, 99%), DMEM-HG cell culture medium and RPMI-1640 cell culture medium were purchased from Sigma-Aldrich (Sintra, Portugal). Fetal bovine serum (FBS) was from Gibco (Thermo Fisher Scientific, Inc., Waltham, MA, USA). All the other reagents were of analytical grade.
5
Synthesis and Characterization of Pd(II)-Spermine Complex
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Cisplatin (cis-dichlorodiammine platinum (II), 99.9%), potassium tetrachloropalladate (II) (K2PdCl4, 98%) and spermine (N,N′-bis(3-aminopropyl)-1,4-diaminobutane, 99%) were purchased from Sigma-Aldrich (Sintra, Portugal). Euthasol® solution (400 mg/mL pentobarbital sodium) was obtained from Le Vet (Oudewater, The Netherlands). All reagents were of analytical grade.
The Pd2Spm complex was synthesized according to published procedures [85 (link),86 (link)]. Briefly, 2 mmol of K2PdCl4 was dissolved in a small amount of water, and 1 mmol of spermine (in aqueous solution) was added dropwise under stirring. After 24 h, the resulting powder was filtered and washed with acetone (yield 68%). The newly synthesized compound was characterized (and tested for purity) by elemental analysis and vibrational spectroscopy [86 (link)].
The Pd2Spm complex was synthesized according to published procedures [85 (link),86 (link)]. Briefly, 2 mmol of K2PdCl4 was dissolved in a small amount of water, and 1 mmol of spermine (in aqueous solution) was added dropwise under stirring. After 24 h, the resulting powder was filtered and washed with acetone (yield 68%). The newly synthesized compound was characterized (and tested for purity) by elemental analysis and vibrational spectroscopy [86 (link)].
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!