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52 protocols using sodium hydroxide (naoh)

1

Synthesis of Multifunctional Nanoparticles

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FeCl3·6H2O, sodium oleate, oleic acid were purchased from Tianjin Yongda Chemical Reagent Co., Ltd.; oleylamine (80–90%) was purchased from Shanghai McLean Biochemical Technology Co., Ltd. Cetyl trimethyl ammonium bromide (CTAB) and ammonium nitrate were purchased from Beijing Chemical Reagent Co., Ltd.; n-hexane, absolute ethyl alcohol and sodium hydroxide (95%) were purchased from Tianjin Damao Chemical Reagent factory; octadecene, N-(2-aminoethyl)-3-amopropyl trimethoxysilane (EDS), tetraethoxysilane (TEOS) were purchased from Beijing Balinwei Reagent Co., Ltd.; Polyoxyethylene-polypropylene-polyoxyethylene copolymer (F127) was purchased from Germany BASF Company; chloroauric acid (HAuCl4·3H2O, 99.99%) was purchased from Alfa Aesha (China) Chemical Co., Ltd.; folic acid (FA, ≥97%), doxorubicin hydrochloride (DOX, ≥98%) and S-Nitrosylglutathione (GSNO) was obtained from Aladdin Bio-chem Technology Co., Ltd.; Griess reagent Shanghai Biyuntian Biotechnology Co., Ltd. 1-hydroxybenzotriazole (HOBT) and O-benzotriazole - tetramethyl urea hexafluorophosphate (HBTU) were purchased from Gill Biochemical (Shanghai) Co., Ltd. All chemicals were analytical reagent grade and used without further purification.
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2

Phenolic Foam Synthesis Protocol

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Phenol, paraformaldehyde, p-toluenesulfonic acid (as a catalyst and hardener), sodium hydroxide (as a catalyst), and n-pentane (as a foaming agent) were purchased from the Tianjin Damao Chemical Reagent Factory (Tianjin, China). Terephthalyl alcohol was purchased from Zhengzhou Alpha Chemical Co., Ltd. (Zhengzhou, China). Tween-80 (as a surfactant) was purchased from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). The raw materials mentioned above are all analytical reagent.
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3

Quinoa Bran Extraction and Analysis

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Quinoa bran (variety: gerbera; origin: Qinghai) was stored at 4°C for use. Petroleum ether, hydrochloric acid, sodium hydroxide, and zinc sulfate heptahydrate were procured from Tianjin Damao Chemical Reagent Factory. Citric acid was purchased from Beijing Beihua Fine Chemicals Co, Ltd. All other reagents were of analytical grade.
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4

Antioxidant and Enzyme Inhibitory Assays

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Ethanol, n-hexane, and ethyl acetate were purchased from Guangdong Guanghua Sci-Tech Co., Ltd. (Shantou, China). Potassium dihydrogen phosphate, dipotassium hydrogenphosphate, ascorbic acid (≥99.0%), trichloroacetic acid, Iron(III) chloride (FeCl3), starch, and sodium hydroxide were purchased from Damao Chemical Reagent Factory (Tianjin, China). Phloroglucinol (≥99.0%), sodium carbonate, diammonium salt (ABTS), α-glucosidase, α-amylase, 3,5-dinitro salicylic acid, and potassium sodium tartrate were purchased from Shanghai Aladdin Biochemical Technology Co., Ltd. (Shanghai, China). 4-nitrophenyl-α-D-glucopyranoside (PNPG), acarbose, 2,2-diphenyl-1-picrylhydrazyl radical (DPPH), and Folin-Ciocalteu reagent were purchased from Beijing Solarbio Technology Co., Ltd. (Beijing China). Potassium ferricyanide and potassium persulfate were purchased from Xilong Science Co., Ltd. (Shantou, China). Methanol was chromatographic grade and purchased from Concord Technology (Tianjin, China).
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5

Synthesis and Characterization of Silica Nanoparticles

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Methanol, ethanol, ethyl acetate, sodium hydroxide, hydrochloric acid, N, N-dimethylformamide, and dimethyl sulfoxide were purchased from Tianjin Damao Chemical Reagent Factory (Tianjin, China). Ethyl orthosilicate, cetyl trimethyl ammonium bromide, 3-aminopropyltriethoxysilane, ammonia water, SA, sodium dihydrogen phosphate, and sodium monohydrogen phosphate were purchased from Aladdin Reagent Co., Ltd. (Shanghai, China). Gen was purchased from Shanghai Macleans Biochemical Technology Co., Ltd. (Shanghai, China).
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6

Characterization of DOM Sources

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Anthracene (99.0%) and pyrene (97.0%) were from Shanghai McLean. Sodium hydroxide (NaOH) and acetonitrile were from Tianjin Damao Chemical Reagent Factory for analytical purity. Deionized water was prepared with Millipore Milli-Q system. Suwannee River fulvic acid Standard II (SRFA), Upper Mississippi River NOM (UMRN) are derived from water source DOM, lliott Soil Humic Acid Standard IV (ESHA), Leonardite Humic Acid Standard (LHA) are from land source DOM which were purchased from the International Humic Acid Association.
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7

Synthesis of Polyelectrolyte Hydrogels

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Allyl polyoxyethylene ether 600 (APEG600) (Tianjin Damao Chemical Reagent Factory, Tianjin, China); acrylic acid (AA) (Tianjin Damao Chemical Reagent Factory); sodium p-styrene sulfonate (SSS) (Aladdin, Hong Kong, China); dimethyldiallyl ammonium chloride (DMDACC); sodium bisulfite (Tianjin Damao Chemical Reagent Factory); potassium persulfate (Tianjin Damao Chemical Reagent Factory); sodium hydroxide (Tianjin Damao Chemical Reagent Factory); potassium bromide (Tianjin Damao Chemical Reagent Factory); deuterated water (Shanghai Maclean Biochemical, Shanghai, China); and ethanol (Tianjin Damao Chemical Reagent Factory) were used in the study.
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8

Phenol-based Rigid Foam Synthesis

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Phenol, paraformaldehyde, sodium hydroxide and n-pentane (as a blowing agent) were purchased from the Tianjin Damao Chemical Reagent Factory (Tianjin, China). As the catalyst, sodium hydroxide was dissolved in distilled water to create a saturated solution before use. We obtained 3-pentadecyl-Phenol from Tianjin Heowns Biochemical Technology Co., Ltd. (Tianjin, China). The above-mentioned raw materials and reagents were all analytical reagents (≥99.7%). Tween-80 (as a surfactant) and benzenesulfonic (as a curing agent) were supplied by Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). Both reagents are chemically pure (≥99.5%).
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9

Synthesis of Polymer-Based Compounds

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CMC (2500–4500 mPa.s); PVA (Mw = 205,000); βCD (98%); and ECH were purchased from Aladdin Biochemical Technology Co., Ltd. Further, sodium hydroxide, sodium thiosulfate, potassium iodide, and potassium dichromate were obtained from the Tianjin Damao Chemical Reagent Factory). The materials were used as obtained without further purification.
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10

Synthesis of Acetoacetic Ester-Terminated Polyether

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Phenol, paraformaldehyde, sodium hydroxide (as a catalyst), n-pentane (as a blowing agent), and ethyl acetoacetate were purchased from the Tianjin Damao Chemical Reagent Factory (Tianjin, China). The above-mentioned raw materials and reagents were all analytical reagents (≥99.7%). Tween-80 (chemically pure, as a surfactant), hydrochloric acid (guaranteed reagent, as a catalyst), and 98% sulfuric acid (as a curing agent) were supplied by Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). Polyether diols (1000D) were supplied by Guangzhou Desson Chemical Co., Ltd. (Guangzhou, China). ethyl acetoacetate and polyether diols were used as raw materials for the synthesis of the acetoacetic ester-terminated polyether.
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