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338 protocols using tga q500

1

Thermogravimetric Analysis Using TA Instruments

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Example 11

Thermogravimetric analysis (TGA) was conducted using a TA Instruments TGA Q500 or Q5000 at a heating rate 10° C./min. The instrument was calibrated using a standard weight for the balance, and Alumel and Nickel standards for the furnace (Curie point measurements). Thermal events such as weight-loss are calculated using the Universal Analysis 2000 software, version 4.1D, Build 4.1.0.16.

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2

Thermal Gravimetric Analysis of Compound I

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Example 15

Thermal Gravimetric Analysis (TGA) was performed on the TA Instruments, Inc. TGA Q500. The instrument is calibrated by the vendor at 10° C./min. for temperature using the curie point of a ferromagnetic standard. The balance is calibrated with a standard weight. Sample scans are performed at 10° C./min. Sample was placed into an open sample pan, previously tared on the TGA balance. Thermal events such as weight-loss are calculated using the Universal Analysis 2000 software, version 4.1D, Build 4.1.0.16.

The TGA thermogram for Form I of 1-[3-(4-bromo-2-methyl-2H-pyrazol-3-yl)-4-methoxy-phenyl]-3-(2,4-difluoro-phenyl)-urea (Compound I) is shown in FIG. 24.

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Biodegradable Film Thermal Stability

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The effect of heat treatment on the biodegradable films was determined using TGA. The thermogravimetric analyzer TGA Q500 (TA Instruments, New Castle, DE, USA) was used. The test conditions were as follows: temperature 30–600 °C at a heating rate of 10 °C·min−1, in a nitrogen atmosphere (50 cm3·min−1).
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4

Thermogravimetric Analysis of Materials

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TGA measurements were performed on a TGA Q500 from T.A. Instruments® (weighting precision of ± 0.01%, 0.1 µg sensitivity) at a heating rate of 10 °C/min from 40 °C to 700 °C or 800 °C, under N2 atmosphere, and a rate of 10 °C/min from 40 °C to 800 °C under O2 atmosphere, in a platinum crucible.
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5

Thermal Stability Analysis of Mycelia

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A thermogravimetric analysis (TGA) was performed using a TGA Q500 (TA Instruments) to assess the mass loss and nature of the species evolved during thermal decomposition, as well as the thermal stability of mycelia. Measurements were performed on 5–8 mg samples in an aluminum pan under an inert N2 atmosphere, with a flow rate of 50 mL/min, over a temperature range of 30°C–600°C, with a 5°C/min heating rate. The weight loss and its derivative were recorded simultaneously as a function of time/temperature.
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Quantifying Nanoparticle Functionalization via TGA

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Thermogravimetric analyses (TGA) were performed in order to estimate the degree of functionalization of the nanoparticles both with APTES and with the GalNAc cluster. This technique is a destructive analysis in which the weight loss of the sample is monitored while it is heated along the desired temperature range. All the tests were conducted on a TGA Q500 (TA Instruments, New Castle, DE, USA). During the measurements, the samples were heated from room temperature to 600 °C at a heating rate of 10 °C/min under a nitrogen atmosphere.
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7

Thermal Gravimetric Analysis of Extruded Filaments

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Thermal gravimetric analysis (TGA) TGA analysis for the extruded filaments was carried out using a TGA Q500 (TA Instruments, Hertfordshire, UK). The filaments were cut into small pieces (<1mm, approximately 10 mg) were accurately weighed and placed in a 40 µL aluminium pan (TA Instruments, Hertfordshire, UK), which was placed on a platinum pan. Samples were then scanned from 25 to 500 o C at a heating rate of 10 o C/min with a nitrogen purge of 40/60 mL/min for the sample and furnace, respectively. All measurements were carried out in triplicates and the data analysed using a TA Universal Analysis 2000 software (TA Instruments, Hertfordshire, UK)
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8

Characterization of Hydrogel Composites

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Dried and pounded hydrogels powder was pressed with KBr and Fourier-transform infrared (FTIR) spectra of the composite hydrogels were recorded with a Bruker Tensor 27 DTGS spectrometer at a wavenumber range of 4000-600 cm -1 with a resolution of 2 cm -1 . The spectra were normalized by height before spectra subtraction was performed.
Thermal stability of the samples was studied by Thermogravimetric Analysis (TGA) using the TGA Q-500 (TA Instruments) equipment. TG traces were registered in the temperature range from 298 to 1073 K at a heating rate of 20 K•min -1 at continuous evacuation of volatile products of degradation.
The swelling ability of gels in a free state at isothermic regime 291±1 K was studied by immersion of dried samples in distilled water (pH = 6.6) and in buffer solution (Na 2 B 2 O 4 ×10H 2 O, pH = 9.18). The sample was placed in the swelling solution and the weight of the swollen sample was measured along the sample exposition periodically taking out and weighting the sample (time of measuring was <1 min). Before weighting the excessive surface liquid was gently removed by filter paper. The degree of swelling (W t ) for each sample at time t was calculated using equation:
where m t and m 0 are the sample weight at any given time, and in the initial dry state, respectively.
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9

Characterization of Dendrimer Nanostructures

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All NMR spectra of synthesized dendrimers were recorded using a Bruker Avance NMR Spectrometer (1H, 300 MHz and 13C, 75 MHz). The spectra were obtained from a DMSO-d6 solution of the complexes with the chemical signals referenced to the solvent residual signal in ppm. Attenuated total reflection Fourier-transform IR (ATR-FTIR) spectroscopic measurements were achieved on a Bruker Alpha FTIR spectrometer Alpha-P using KBr pellet technique in the wavenumber range between 4000 to 400 cm−1. Elemental carbon and hydrogen analyses for prepared dendrimers were performed on CE-440 Elemental Analyser, Exeter Analytical. Thermogravimetric analysis (TGA) was conducted in platinum pans under nitrogen at a heating rate of 10 °C on a TA Instruments TGA Q500.
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10

SPION Characterization by TGA

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The amount of oleic acid coating on the SPION and the weight percentage of SPION in m-NC were characterised by the thermogravimetric analysis (TGA) using TGA Q500 (TA instrument), where about 10 mg of SPION was loaded into platinum pan. The measurement was pre-equilibrated at 100 °C and then heated from 100 °C to 1000°C with a temperature ramp of 10 °C/min under compressed air atmosphere with balance and sample purge flow at 10 and 90 ml/min, respectively.
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