Nitrogen filled glovebox

Manufactured by MBraun

The Nitrogen-filled glovebox is a laboratory equipment designed to create and maintain an inert, oxygen-free environment for sensitive materials and processes. The glovebox uses nitrogen gas to displace oxygen, providing a controlled and isolated workspace.

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Glovebox (35 citations)

2 protocols using nitrogen filled glovebox

Synthesis of Amphiphilic NHC Iron Complex

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All reactions were carried out under nitrogen
in a nitrogen-filled glovebox (MBraun) or using common Schlenk techniques.
THF and diethyl ether were distilled from sodium/benzophenone ketyl.
Dichloromethane was distilled from CaH₂. The solvents were
degassed by repetitive freeze/pump/thaw cycles and stored under dry
nitrogen or argon. All other reagents were commercial grade and used
as received. The amphiphilic NHC precursor (1)^{19 (link)} and FeCl₂(thf)_1.5^{26 (link)} were prepared according to literature procedures.

Donner A., Trepka B., Theiss S., Immler F., Traber J, & Polarz S. (2019). NHC-Metallosurfactants as Active Polymerization Catalysts. Langmuir, 35(50), 16514-16520.

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Inert Atmosphere Synthesis and Handling

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With the exception of the starting materials, all reactions and manipulations were carried out under an atmosphere of dry, O₂-free nitrogen using standard double-manifold techniques with a rotary oil pump. A nitrogen-filled glove box (MBraun) was used to manipulate solids including the storage of starting materials, room temperature reactions, product recovery and sample preparation for analysis. All solvents (CH₂Cl₂, hexane, pentane) were dried by employing a solvent purification system MB SPS-800 and stored under a nitrogen atmosphere. Deuterated solvents were distilled and/or dried over molecular sieves before use. Chemicals were purchased from commercial suppliers and used as received.

Wilkins L.C., Santi N., Luk L.Y, & Melen R.L. (2017). Reactions of biologically inspired hydride sources with B(C6F5)3. Philosophical transactions. Series A, Mathematical, physical, and engineering sciences, 375(2101), 20170009.

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