LC-MS grade solvents used for method development (water and methanol) were purchased from Burdick and Jackson (Muskegon, MI). All reference and internal standards except levofloxacin, bedaqualine, ethionamide-d5, prothionamide-d5, and bedaquiline-d6 were purchased from Toronto Research Chemicals (Toronto, ON). Reference standards for levofloxacin and bedaquiline were purchased from Sigma (St Louis, MO). Ethionamide-d5, prothionamide-d5, and bedaquiline-d6 were purchased from ClearSynth (Mississauga, ON). Formic acid solution was purchased from Sigma (St Louis, MO).
Bedaquiline d6
Manufactured by LGC
Sourced in Canada
Bedaquiline-d6 is a stable-isotope labeled compound used as an internal standard in analytical methods for the quantification of bedaquiline, an antibiotic medication used to treat tuberculosis. Bedaquiline-d6 contains six deuterium atoms, which allow it to be distinguished from the unlabeled bedaquiline molecule during mass spectrometric analysis. This compound is often employed in liquid chromatography-mass spectrometry (LC-MS) assays to ensure accurate and precise measurements of bedaquiline concentrations in biological samples.
Automatically generated - may contain errors
Lab products found in correlation
Bedaquiline, by Merck Group (1 mentions)
Formic acid solution, by Merck Group (1 mentions)
Levofloxacin, by LGC (1 mentions)
Levofloxacin, by Merck Group (1 mentions)
Lc ms ms grade millipore water, by Merck Group (1 mentions)
Dimethyl sulfoxide (dmso), by Merck Group (1 mentions)
Formic acid, by Merck Group (1 mentions)
Acetone, by Honeywell (1 mentions)
Acetonitrile, by Honeywell (1 mentions)
2 protocols using bedaquiline d6
1
Analytical Method for Antimicrobial Drugs
2
Analytical Workflow for Bedaquiline Quantification
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Bedaquiline reference material and the internal standard, bedaquiline-d6, were purchased from Toronto Research Chemicals (Ontario, Canada), while M2 was purchased from Clearsynth (Mumbai, India), and M2-d3-13C was donated by Janssen (Beerse, Belgium). Methanol and trifluoroacetic acid (TFA) were purchased from Anatech (Gauteng, SA) and Sigma-Aldrich (Missouri, USA), respectively. Acetone and acetonitrile were purchased from Honeywell (North Carolina, USA). Formic acid and dimethyl sulfoxide (DMSO) were purchased from Merck (Darmstadt, Germany). LC-MS/MS grade Millipore water was sourced in-house (Merck-Millipore, Germany).
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