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Diethylamine

Manufactured by Fujifilm
Sourced in Japan

Diethylamine is a chemical compound used in various laboratory applications. It serves as a reagent and solvent, facilitating chemical reactions and analytical procedures. The core function of diethylamine is to provide a basic, alkaline environment for specific laboratory processes. No further details or interpretations can be provided within the given constraints.

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2 protocols using diethylamine

1

Synthesis of IL 1 with Diethylamine

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The chemical reaction between IL 1 and diethylamine (Wako Pure Chemical Industries, Ltd., Osaka, Japan) was performed without any catalyst. First, 2 mmol of diethylamine was added to 1 mmol of IL 1 in 1 mL of ethanol. The mixture was stirred for 24 h at 343 K in an airtight test tube in an air atmosphere (Scheme 3c). After the reaction was complete, the extra diethylamine and ethanol were evaporated from the mixture. The residual solvent was removed from the mixture by drying thoroughly in vacuo. The product was confirmed by mass spectrometry. HRMS (FAB), m/z: calcd for C32H62F6N5O6S2+ 790.4040 [M + C15H31N2O]+; found 790.4048.
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2

Derivatization and HPLC Analysis of Amino Acids

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Amino acids (L-serine, L-alanine, L-valine, and L-proline), sodium hydroxide, sodium tetraborate, citric acid, sodium perchlorate monohydrate and diethylamine were purchased from Wako Pure Chemical Industries, Ltd. (Osaka, Japan). The 4-Fluoro-7-nitro-2,1,3-benzoxadiazole (NBD-F) was obtained from Dojindo Laboratories (Kumamoto, Japan). Chloro(dimethyl)octadecylsilane, 95% (ODS-Cl), was obtained from Sigma-Aldrich (St. Louis, MO). Toluene and acetonitrile were of HPLC grade and were obtained from the Kanto Chemical Co., Inc. (Tokyo, Japan). Water was purified using a Milli-Q system (Millipore, Bedford, MA).
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