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3flex surface characterisation analyser

Manufactured by Micromeritics
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The 3Flex surface characterization analyzer is a versatile and automated instrument designed for the measurement of surface area, pore size, and pore volume of solid materials. It utilizes the physical adsorption of gases, such as nitrogen, argon, or carbon dioxide, to provide accurate and reliable data on the surface and pore properties of a wide range of materials, including catalysts, adsorbents, and nanomaterials.

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Lab products found in correlation

Spectrum two ir, by PerkinElmer (1 mentions) Ultra plus microscope, by Zeiss (1 mentions)

2 protocols using 3flex surface characterisation analyser

1

Textural Characterization of Adsorbent Materials

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The adsorption-desorption isotherms were recorded at 77 K using a Micromeritics 3Flex surface characterisation analyser. The samples were degassed in vacuum at 200 °C overnight for removal of any adsorbates. Specific surface areas were determined according to the BET model.
Kang L., Wang B., Bing Q., Zalibera M., Büchel R., Xu R., Wang Q., Liu Y., Gianolio D., Tang C.C., Gibson E.K., Danaie M., Allen C., Wu K., Marlow S., Sun L.D., He Q., Guan S., Savitsky A., Velasco-Vélez J.J., Callison J., Kay C.W., Pratsinis S.E., Lubitz W., Liu J.Y, & Wang F.R. (2020). Adsorption and activation of molecular oxygen over atomic copper(I/II) site on ceria. Nature Communications, 11, 4008.
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2

Multimodal Characterization of MIL-53(Al)

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Attenuated total reflectance-Fourier transform infrared (ATR-FTIR) spectra were recorded for MIL-53(Al) on a PerkinElmer Spectrum Two IR spectrometer (with UATR Two attachment). TGA measurements were carried out on a DISCOVERY TGA Thermogravimetric Analyzer. Approximately 5 mg of each sample was placed on a platinum pan which was heated under a flow of air at a rate of 10 °C min–1 up to 700 °C. Field-emission SEM (FE-SEM) images were obtained using a Zeiss ULTRA plus microscope (working distance ∼9 mm; acceleration voltage 20 kV). N2 sorption isotherms were recorded on a 3Flex Surface Characterisation Analyser (Micromeritics Instruments Inc.).
Liang W., Li L., Hou J., Shepherd N.D., Bennett T.D., D'Alessandro D.M, & Chen V. (2018). Linking defects, hierarchical porosity generation and desalination performance in metal–organic frameworks †Electronic supplementary information (ESI) available. See DOI: 10.1039/c7sc05175a. Chemical Science, 9(14), 3508-3516.
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