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135 protocols using nicolet 5700

1

Characterization of Latex Particles

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The latex particles size data of latex particles were obtained from dynamic light scattering on a Malvern particle size (PSD; Nano-ZS90, Malvern Panalytical, Almelo, The Netherlands).
GPC (gel permeation chromatography) analysis was performed in THF (tetrahydrofuran) (1.0 mL/min, 30 °C) while using a Viscotek TDA302 (GPC; Viscotek TDA302, Malvern Panalytical, Almelo, The Netherlands) with a WL. M GPC solvent/sample module.
FTIR (Fourier transform infrared spectroscopy) analyses were obtained from Nicolet 5700 (FTIR; Nicolet 5700, Thermo Electron Co., Waltham, MA, USA) within the frequency range of 650–4000 cm−1 by KBr pellets technique and a resolution of 4 cm−1 was used to analyze the chemical structure of the dried latex particles.
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Comprehensive Characterization of Optoelectronic Devices

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UV-1800 (SHIMADZU Co., Japan) was used to measure the UV-vis absorbance of TFB films, and Nicolet5700 (Thermo electron Co., USA) was used to measure the FT-IR absorbance peaks of TFB films. M6100 OLED I-V-L Test System (McScience Co., Korea) was used to measure the current - voltage - luminance (IVL) and current density - voltage (CD - V) characteristics of QLEDs and HODs, respectively. Agilent 4284a Precision LCR meter (Agilent technologies, USA) was used to measure the capacitance - frequency (C-f) and capacitance - voltage (C-V) characteristics of the HODs.
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Characterization of Polymer Coatings for Biomedical Applications

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The morphologies of bare 316L SS, PTMC and PTMC-E5 samples were observed by scanning electron microscopy (SEM, JSM-7001F, Japan Electron Optics Laboratory Co., Ltd., Tokyo, Japan), and the surface chemical composition of PTMC-E5 was examined using Fourier transform infrared spectrometry (FTIR, NICOLET 5700, Thermo Electron Corporation, Waltham, MA, USA) with reflectance mode and X-ray photoelectron spectroscopy (XPS, K-Alpha, Thermo Electron Limited, Winsford, UK) [29 (link),30 (link),31 (link)]. The wettability of the bare 316L SS, PTMC and PTMC-E5 sample surfaces was assessed by water and blood contact angle measurement (DSA 100, Krüss GmbH, Hamburg, Germany) [32 (link)]: the samples were first dried and then fixed to a glass slide. A droplet of dH2O was added to the surface to detect contact angle using a horizontal microscope. For each sample, the mean value of the contact angle was calculated from at least three individual measurements taken at different locations on the samples examined. The drug-eluting portion of the estradiol was also investigated, as described elsewhere [16 (link)].
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Characterization of Activated Carbon

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The specific surface area and pore distribution of OS-CS AC were characterized by BET analysis (ASAP-2020-HD88, American Mike Instrument Company), and the data were analysed using Origin2018 software. The crystal structures of the OS-CS AC were characterized using an X-ray polycrystalline diffractometer (D8 Advance, Bruker Instruments, Germany), and the data were collected in the angle range of 10–80 (2θ). Scanning electron microscopy (SEM) (EM-30 Plus, Kusem Instrument Company) was used to detect the microstructure and pore distribution of the OS-CS AC. X-ray photoelectron spectroscopy (XPS; EscaLab 250Xi, China) was performed to determine the adsorption of Cr(VI) and Cr(III) on the surface of OS-CS AC, and the data were analysed using Avantage2018 software. An elemental analyser (EAI, German Elemental Analysis System Company) was used to detect the basic properties of OS and CS. The functional groups on the OS-CS AC surface were characterized using a Fourier transform infrared spectrometer (FTIR; Nicolet 5700, Thermo Electron Corporation) and Boehm titration33 (link).
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5

FTIR Analysis of Film Composition

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The chemical composition of the films was observed by FTIR (Nicolet 5700, Thermo Electron, Hampton, NH, USA) from 4000 to 600 cm−1 at a scanning rate of 4 cm−1. The samples were fixed directly in the sample holder and evaluated.
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6

Characterization of Zinc-Doped Hydroxyapatite

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The phase composition of the Zn-HA was characterized by X-ray diffraction (XRD) (X'Pert PRO MPD, PANalytical Ltd., Almelo, Netherlands). The diffraction pattern was analysed over a 2θ range of 20°–70°, using CuKa radiation (λ = 1.54056 Å). A 40 kV voltage was applied to the X-ray tube, while the current intensity was 40 mA. The XRD data were then analysed using MDI Jade 5.0 and X'Pert HighScore 1.0 (Philips, Netherlands). The chemical characterization of Zn-HA was performed by Fourier transformed infrared spectroscopy (FTIR) (Nicolet 5700, Thermo Electron, USA) spectrophotometer in the region of 400–4,000 cm−1 on powder samples pelleted in a KBr matrix with spectral resolution of 4 cm−1. The chemical composition analysis of Zn-HA was performed by energy dispersive spectrometer (EDS) (Inca Penta FETX3, Oxford, UK) with MgKa radiation (1,253.6 eV) operating at 100 W.
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7

Functional Group Analysis of IEMs

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The functional groups of the IEMs were detected using an attenuated total reflectance-Fourier transform infrared (ATR-FTIR) spectrometer (Nicolet 5700, Thermo Electron Corporation, USA), and all the spectra were collected with OMNIC 8.0 software. The membrane samples were dried in a 38 °C oven for 24 h for complete drying prior to the measurement.
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8

Algae Infrared Spectroscopy Preparation

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The infrared spectra of the algae were obtained using a Fourier transform infrared spectrometer (NICOLET 5700, Thermo Electron Corporation). For the FTIR study, 30 mg of the biomass was encapsulated in 300 mg of KBr (Sigma) in order to prepare translucent sample disks.
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9

FTIR Analysis of PrP Fibrils

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Attenuated total reflection FTIR spectra of PrP fibril samples were recorded using a Nicolet 5700 FTIR spectrophotometer (Thermo Electron, Madison, WI), as described in detail previously [27] (link). Briefly, 3 ml PrP fibril samples were harvested (∼150000 g) within a time range of the plateau of each kinetic curve of ThT fluorescence, and then washed by H2O and dried by vacuum drying. The dried samples were prepared in D2O and FTIR spectra were recorded in the range from 400 to 4000 cm−1 at 4 cm−1 resolution. The sample was scanned 32 times in each FTIR measurement, and the spectrum acquired is the average of all these scans. Spectra were corrected for the D2O and water vapors. Measurements were made at 25°C.
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10

Characterization of Organic Groups in AFP

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A Thermo Nicolet 5700 infrared spectrophotometer (Thermo Electron, Madison, WI, USA) was used to characterize the organic functional groups of AFP using the KBr-pellets method, with the range of 400–4000 cm−1 [29 (link)].
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