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3 4 ethylenedioxythiophene

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3,4-ethylenedioxythiophene is a chemical compound used in the production of conductive polymers. It serves as a key material in the manufacturing of electronic components and devices.

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Lab products found in correlation

Nitromethane, by Thermo Fisher Scientific (2 mentions) Triethylamine, by Thermo Fisher Scientific (2 mentions) Magnesium sulfate, by Avantor (1 mentions) Iron 3 chloride, by Thermo Fisher Scientific (1 mentions) Tetrahydrofuran, by Lach-Ner (1 mentions) Dichloromethane, by Lach-Ner (1 mentions) Chloroform, by Lach-Ner (1 mentions) Ammonium hydroxide, by Lach-Ner (1 mentions) Dibutyltin dilaurate, by Thermo Fisher Scientific (1 mentions) Methanol, by Carlo Erba (1 mentions) Aniline, by Chempur (1 mentions) Sodium polystyrene sulfonate, by Merck Group (1 mentions) Graphite foil, by Thermo Fisher Scientific (1 mentions) Pyrrole, by Thermo Fisher Scientific (1 mentions) Sodium chloride (nacl), by ITW Reagents (1 mentions) Glucose glu, by Thermo Fisher Scientific (1 mentions) Myoglobin myo, by Merck Group (1 mentions) 4 aminothiophenol, by Thermo Fisher Scientific (1 mentions) Phosphate buffered saline tablet, by Merck Group (1 mentions) Immunoglobulin g igg, by Merck Group (1 mentions)

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3,4-ethylenedioxythiophene (EDOT, (2 citations)

5 protocols using 3 4 ethylenedioxythiophene

1

Organic Synthesis Reagents Database

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Dichloromethane (CH2Cl2), chloroform (CHCl3, 99.94%), tetrahydrofuran (THF) (C4H8O, 99.94%) and ammonium hydroxide (NH4OH, 24.06%) were received from Lach-Ner s.r.o., Neratovice, Czech Republic. α-bromoisobutyryl bromide (C4H6Br2O, >98.0%), 3-thiopheneethanol (C6H8OS, 98.0%) and N,N,N′,N″,N″-pentamethyldiethylenetriamine (PMDETA) (C9H23N3, >99.0%) were recieved from Tokyo Chemical Industry, Tokyo, Japan. Nitromethane (CH3NO2, 98+%), copper(I) bromide (CuBr, 98%), dibutyltin dilaurate (DBTDL, [CH3(CH2)3]2Sn[O2C(CH2)10CH3], iron(III) chloride, anhydrous (FeCl3, 98%) and ethyl isocyanate (C3H5NO, 98%) were received from Alfa Aesar, Haverhill, MA, USA. Triethylamine (C6H15N, 99%), 3,4-ethylenedioxythiophene (EDOT, 99.0%) silica gel (SiO2) and 2-hydroxyethyl acrylate (C5H8O3, 97%) were received from Acros Organics, Geel, Belgium. Magnesium sulfate (MgSO4, 99.4%) was received from VWR Chemicals, Leuven, Belgium. Acetone (C3H6O, 98.0%) and ethanol (C2H5OH, 96.0%) were received from Gram-mol, Zagreb, Croatia. Methanol (CH3OH, 99.9%) was received from Carlo Erba Reagents, Val-de-Reuil, France and diethyl eter (C4H10O) was received from Macron Fine Chemicals, Radnor, PA, USA. All the solvents were used as received.
Fiket L., Božičević M., Brkić L., Žagar P., Horvat A, & Katančić Z. (2022). Intrinsically Stretchable Poly(3,4-ethylenedioxythiophene) Conducting Polymer Film for Flexible Electronics. Polymers, 14(12), 2340.
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2

Synthesis and Characterization of Thiophene-Based Materials

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All chemical reagents were used as received without any purification. 3-tiopheneethanol (97%), triethylamine (99%), 3,4-ethylenedioxythiophene (98%), silica gel, and nitromethane (99+%) were purchased from Acros Organics, Geel, Belgium. Methanol (MeOH, p.a.), dichloromethane (DCM, p.a.), ammonium hydroxide, and chloroform (CHCl3, p.a.) were purchased from Lach-Ner s.r.o., Neratovice, Czech Republic. Iron (III) chloride (FeCl3, 98%, anhydrous) was obtained from Alfa Aesar, Havernhill, MA, USA, and α-bromoisobutyril bromide (BiBB, 98%) from Tokyo Chemical Industry, Tokyo, Japan.
Božičević M., Fiket L., Vujasinović M., Blažic R., Kovačić M, & Katančić Z. (2023). Investigation of the Conditions for the Synthesis of Poly(3,4-ethylenedioxythiophene) ATRP Macroinitiator. Polymers, 15(2), 253.
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3

Conductive Polymer Composite Synthesis

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Aniline (p.a. Chempur, Karlsruhe, Germany), sodiumpolystyrene sulfonate (Sigma Aldrich, Saint Louis, MO, USA) and 3,4-ethylenedioxythiophene (99%, Acros Organics, Geel, Belgium) were used as received. Sulfuric acid (p.a. 95%) and hydrochloric acid (p.a. 35%), used for electrolyte preparation, were purchased from POCH. Graphite foil (thickness 0.4 mm, 99.8%, Alfa Aesar, Haverhill, MA, USA) was used as the conductive substrate.
Zarach Z., Trzciński K., Łapiński M., Lisowska-Oleksiak A, & Szkoda M. (2020). Improving the Performance of a Graphite Foil/Polyaniline Electrode Material by a Thin PEDOT:PSS Layer for Application in Flexible, High Power Supercapacitors. Materials, 13(24), 5791.
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4

Synthesis and Characterization of PEDOT:PSS

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Pyrrole (Py, MW 67.09g/mol) and dopant poly (sodium-p-styrenesulfonate) (PSS, MW 70kg/mol) was purchased from Acros-Organics. 3,4-Ethylenedioxythiophene (EDOT) was purchased from Alfa Aesar. N-type Si wafers coated with SiO2 were purchased from University Wafer Company. Stainless Steel wafer masks were designed in house and purchased after fabrication by PhotoEtch Company. All other materials and reagents were used as purchased.
Antensteiner M, & Abidian M.R. (2017). Tunable Nanostructured Conducting Polymers for Neural Interface Applications. Conference proceedings : ... Annual International Conference of the IEEE Engineering in Medicine and Biology Society. IEEE Engineering in Medicine and Biology Society. Annual Conference, 2017, 1881-1884.
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5

Electrochemical Biosensor Protocol

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All chemicals were of analytical grade and ultrapure Milli-Q water laboratory grade (conductivity b0.1 μS/cm) was used. The chemical reagents used included potassium hexacyanoferrate (III) (K 3 [Fe(CN) 6 ]) and potassium hexacyanoferrate (II) trihydrate (K 4 [Fe(CN) 6 ].3H 2 O), obtained from Riedel-de Häen; Phosphate buffered saline (PBS) tablets purchased from Sigma-Aldrich; 3,4-Ethylenedioxythiophene, 97% (EDOT), from Alfa Aesar; 4-Aminothiophenol, 96% (4-AMP), from Acros Organics; EriochromeBlack T (EBT), from Biochem; Interleukin-1β (IL-1β) (AA 117-269) with purity N95% in PBS pH 7.4 (concentration 1 mg/mL) from Antibodies-online, Germany. Myoglobin (Myo) and Immunoglobulin G (IgG) were purchased from Sigma-Aldrich; Glucose (Glu) from Fisher BioReagents and Urea from Fagron; sodium chloride (NaCl) from Panreac; potassium chloride (KCl) and calcium chloride (CaCl 2 ) from Merck; magnesium chloride hexa-hydrate (MgCl 2 .6H 2 O) from Riedel-de Häen was also used.
Cardoso A.R., de Sá M.H, & Sales M.G.F. (2019). An impedimetric molecularly-imprinted biosensor for Interleukin-1β determination, prepared by in-situ electropolymerization on carbon screen-printed electrodes. Bioelectrochemistry (Amsterdam, Netherlands), 130.
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