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4 chlorophenol

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4-chlorophenol is a chemical compound that is used as a reagent and intermediate in various industrial and laboratory applications. It is a crystalline solid with a distinct phenolic odor. 4-chlorophenol serves as a precursor for the synthesis of other chemical compounds and is utilized in research and analytical procedures within the scientific community.

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Lab products found in correlation

Sulfuric acid, by Thermo Fisher Scientific (2 mentions) Palladium catalyst, by Thermo Fisher Scientific (2 mentions) Anhydrous sodium sulfate, by Thermo Fisher Scientific (2 mentions) Benzoic acid, by Thermo Fisher Scientific (2 mentions) Phenol, by Thermo Fisher Scientific (2 mentions) Acetic acid, by Thermo Fisher Scientific (2 mentions) Acetonitrile, by Thermo Fisher Scientific (2 mentions) Sodium bicarbonate, by Thermo Fisher Scientific (2 mentions) 4 hydroxylbenzoic acid, by Thermo Fisher Scientific (2 mentions) O phosphoric acid, by Thermo Fisher Scientific (2 mentions) Palladium catalyst, by Merck Group (2 mentions) Potassium hydrogen phthalate c8h5ko4, by Merck Group (2 mentions) Sodium hydroxide (naoh), by Thermo Fisher Scientific (2 mentions) Milli q system, by Merck Group (2 mentions) Methanol, by Merck Group (2 mentions) Atrazine, by Merck Group (2 mentions) Reactive blue 19, by Merck Group (2 mentions) Methanol, by Thermo Fisher Scientific (2 mentions) Ibuprofen, by Thermo Fisher Scientific (2 mentions) γ al2o3, by Thermo Fisher Scientific (2 mentions)

6 protocols using 4 chlorophenol

1

Catalytic Hydrogenation of 4-Chlorophenol

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4-chloroPhenol (C6H5ClO, 99+ %) and palladium catalyst (Pd/Al2O3, 1% Pd on alumina powder, with a specific surface area of 150 m2g−1) were purchased from Acros and Alfa Aesar, respectively. Phenol (C6H5OH, 89.6%), sodium sulfate anhydrous (Na2SO4, 99%), sulfuric acid (H2SO4, 98%), sodium bicarbonate (NaHCO3, 99–100%), acetonitrile (99.8+ %), sodium hydroxide (NaOH, 96%), benzoic acid (C7H6O2, 99.9+%), 4-hydroxylbenzoic acid (C7H6O3, 99.9+%), o- Phosphoric acid (H3PO4, 85%), and Acetic Acid (Glacial, HPLC grade) were acquired from Fisher Scientific. Ferrous sulfate (FeSO4.7H2O, pro analysis) was obtained from J.T. Baker Analyzed. palladium catalyst (1% on carbon 4 to 8 mesh), Potassium-hydrogen phthalate (C8H5KO4), HPLC grade water, and methanol were bought from Sigma-Aldrich. The syringe filters with 0.22 μm and 0.45 μm pore sizes were purchased from Millex. Titanium sulfate (TiSO4, 65%) was obtained from GFS Chemicals. All solutions were prepared in de-ionized water (18.2 mΩ.cm), obtained from a Millipore Milli-Q system.
Nazari R., Rajić L., Xue Y., Zhou W, & Alshawabkeh A.N. (2018). Degradation of 4-Chlorophenol in Aqueous Solution by Sono-Electro-Fenton Process. International journal of electrochemical science, 13(9), 9214-9230.
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2

Synthesis of Polymeric Biomaterials

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Terephthalic acid (purity ≥99%) was purchased from Acros Organics and butyltin hydroxide oxide hydrate (97%) from Sigma-Aldrich. 1,4-Cyclohexanedimethanol (>99%) with 70% of the trans isomer, dimethyl terephthalate (DMT, >99%) were purchased from TCI. Isosorbide was acquired from Roquette Frères (≥99.9%). 2,5-Furandicarboxylic acid (FDCA, >99.5%) was provided by Avantium.
p-Cresol (4-methyl phenol, >99%), guaiacol (2-methoxy phenol, >99%) and 4-chlorophenol (>99%) were purchased from ACROS Organics, 4-ethyl phenol (98%), 4-methoxyphenol (99%) and dimethoxybenzene (99%) from Sigma Aldrich and 4-ethyl guaiacol (4-ethyl-2-methoxyphenol, 97%) from ABCR.
Bottega Pergher B., Girigan N., Vlasblom S., Weinland D.H., Wang B., van Putten R.J, & Gruter G.J. (2023). Reactive phenolic solvents applied to the synthesis of renewable aromatic polyesters with high isosorbide content. Polymer Chemistry, 14(27), 3225-3238.
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3

FeOCl Nanocatalyst for Fenton-like Treatment

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FeCl3•6H2O (Honeywell Fluka) was used to synthesize the FeOCl nanocatalyst, and H2O2 was purchased from Fisher Scientific. γ-Al2O3 (Alfa Aesar) was used as a support to immobilize FeOCl. BPA (Sigma-Aldrich), ibuprofen (Alfa Aesar), atrazine (Sigma-Aldrich), carbamazepine (Sigma-Aldrich), 4-chlorophenol (Acros Organics), 4-nitrophenol (Acros Organics), rhodamine B (Harleco), reactive blue 19 (Sigma-Aldrich), and orange II (Acros Organics) were used as substrates for the Fenton-like process treatment. Other chemicals (i.e., sodium sulfate [Na2SO4] as the supporting electrolyte, sodium carbonate [Na2CO3] for synthetic alkaline water, ethanol as a HO• radical scavenger, and methanol and acetonitrile as the mobile phase for high-performance liquid chromatography [HPLC]) were purchased from Fisher Scientific. Pure water was used throughout the work, except in the field water studies.
Chen L., Alshawabkeh A.N., Hojabri S., Sun M., Xu G, & Li J. (2021). A Robust Flow-Through Platform for Organic Contaminant Removal. Cell reports. Physical science, 2(1), 100296.
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4

Microtox, Nitrification, and AOP Protocols

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Supplies for Microtox® toxicity testing, such as Microtox® Accute reagent vials, were obtained from Modern Water (New Castle, DE, USA). 4-chlorophenol, 99+% from Acros Organics (Waltham, MA, USA) was used for the Microtox® control. Nitrification inhibition testing utilized the AmVer high range ammonia reagent set (Hach, Loveland, CO, USA), N-allythiourea, 98% from Alfa Aesar (Ward Hill, MA, USA), and ammonium sulfate, granular/certified ACS from Fisher (Waltham, MA, USA). The target chemicals for AOP testing are listed in Table S1, along with their structure, grade, and suppliers. The hydrogen peroxide AOP reagent was 30% w/v, certified ACS from Sigma-Aldrich (St. Louis, MO, USA).
Phillips R.B., James R.R, & Magnuson M.L. (2019). Functional categories of microbial toxicity resulting from three advanced oxidation process treatments during management and disposal of contaminated water. Chemosphere, 238, 124550.
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5

Catalytic Hydrogenation of 4-Chlorophenol

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4-chloroPhenol (C6H5ClO, 99+ %) and palladium catalyst (Pd/Al2O3, 1% Pd on alumina powder, with a specific surface area of 150 m2g−1) were purchased from Acros and Alfa Aesar, respectively. Phenol (C6H5OH, 89.6%), sodium sulfate anhydrous (Na2SO4, 99%), sulfuric acid (H2SO4, 98%), sodium bicarbonate (NaHCO3, 99–100%), acetonitrile (99.8+ %), sodium hydroxide (NaOH, 96%), benzoic acid (C7H6O2, 99.9+%), 4-hydroxylbenzoic acid (C7H6O3, 99.9+%), o- Phosphoric acid (H3PO4, 85%), and Acetic Acid (Glacial, HPLC grade) were acquired from Fisher Scientific. Ferrous sulfate (FeSO4.7H2O, pro analysis) was obtained from J.T. Baker Analyzed. palladium catalyst (1% on carbon 4 to 8 mesh), Potassium-hydrogen phthalate (C8H5KO4), HPLC grade water, and methanol were bought from Sigma-Aldrich. The syringe filters with 0.22 μm and 0.45 μm pore sizes were purchased from Millex. Titanium sulfate (TiSO4, 65%) was obtained from GFS Chemicals. All solutions were prepared in de-ionized water (18.2 mΩ.cm), obtained from a Millipore Milli-Q system.
Nazari R., Rajić L., Xue Y., Zhou W, & Alshawabkeh A.N. (2018). Degradation of 4-Chlorophenol in Aqueous Solution by Sono-Electro-Fenton Process. International journal of electrochemical science, 13(9), 9214-9230.
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6

FeOCl Nanocatalyst for Fenton-like Treatment

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FeCl3•6H2O (Honeywell Fluka) was used to synthesize the FeOCl nanocatalyst, and H2O2 was purchased from Fisher Scientific. γ-Al2O3 (Alfa Aesar) was used as a support to immobilize FeOCl. BPA (Sigma-Aldrich), ibuprofen (Alfa Aesar), atrazine (Sigma-Aldrich), carbamazepine (Sigma-Aldrich), 4-chlorophenol (Acros Organics), 4-nitrophenol (Acros Organics), rhodamine B (Harleco), reactive blue 19 (Sigma-Aldrich), and orange II (Acros Organics) were used as substrates for the Fenton-like process treatment. Other chemicals (i.e., sodium sulfate [Na2SO4] as the supporting electrolyte, sodium carbonate [Na2CO3] for synthetic alkaline water, ethanol as a HO• radical scavenger, and methanol and acetonitrile as the mobile phase for high-performance liquid chromatography [HPLC]) were purchased from Fisher Scientific. Pure water was used throughout the work, except in the field water studies.
Chen L., Alshawabkeh A.N., Hojabri S., Sun M., Xu G, & Li J. (2021). A Robust Flow-Through Platform for Organic Contaminant Removal. Cell reports. Physical science, 2(1), 100296.
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