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Interface 1000e

Manufactured by Gamry
Sourced in United States

The Interface 1000E is a potentiostat/galvanostat product from Gamry. It is designed for electrochemical measurements and analysis. The device provides highly accurate and precise control of potential and current for a variety of electrochemical techniques.

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10 protocols using interface 1000e

1

Electrochemical Characterization of Gel Polymer Electrolytes

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The precursor solution of GPE was prepared in a transparent glass bottle, and two stainless steel plates were inserted below the liquid level. The changes in the conductivity of the system, from flexible precursor solution to immobile GPE, were recorded by an electrochemical workstation (Interface 1000E, Gamry Instruments). The conductivity was calculated by the following equation: G = l/(RS), where l is the distance between two stainless steel plates, R is the resistance value, and S is the effective area below the liquid surface. The LSV curves of GPE and LE were obtained by placing the GPE/LE between a stain steel plate and lithium foil at a sweep rate of 1.0 mV s−1. The CVs of batteries with GPE and LE were measured via the electrochemical workstation (Interface 1000E, Gamry Instruments) in the voltage range of 1.8 to 3.0 V at a scanning rate of 0.05 mV s−1. Electrochemical impedance spectra (EIS) of batteries with GPE and LE were tested by the electrochemical workstation (Interface 1000E, Gamry Instruments) in the frequency range of 10−1 to 105 Hz. The Li|GPE|Li and Li|LE|Li symmetric cells were studied using LAND (LANHE CT2001A) using different current densities. The galvanostatic charge/discharge tests of batteries, including Li-S batteries, Li-LiFePO4 batteries, and Li-NCM622 batteries with GPE and LE were examined using the LAND testing system (LANHE CT2001A).
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2

Electrochemical Impedance Spectroscopy Technique

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The electrochemical impedance spectroscopy experiments were recorded on a Gamry Interface 1000 E potentiostat in potentiostatic mode at open circuit potential in the frequency range 1 Hz to 100 kHz with 10 mV amplitude of the test signal. The data were analyzed with the Gamry instrument version 7.05 package software.
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3

Electrochemical Performance Evaluation of LP-C Sensor

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The electrochemical performance of the LP-C electrochemical sensor was evaluated using a Gamry instrument (Interface 1000E, USA). The LP-C electrode was placed in a 3-electrode cell system as a working electrode with 0.1 M PBS (pH 7.4) with Ag/AgCl as a reference electrode and a Pt wire as a counter electrode. CV over a potential range of −0.1 to 0.6 V and a scan rate of 10 and 50 mV s−1 with 0.1 M PBS (pH 7.4) in the presence of 0.2 mM DA, 5 mM UA and 5 mM AA. Differential pulse voltammetry (DPV) was also measured with the same concentration of analytes and electrolyte over a potential range of −0.1 to 0.5 V and a scan rate of 10 and 50 mV s−1. For the DA concentration study, DPV responses of different DA concentrations in the presence of 20 μM UA and AA were recorded over a potential range of −0.1 to 0.5 V with the following parameters: pulse height of 45 mV, step size of 1 mV, pulse time of 0.03 s, sample period of 0.4 s, and scan rate of 2.5 mV s−1.
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4

Discharge Characterization of NMC111 Coin Cells

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Discharge tests were performed on the assembled coin cells (three repeat tests) at room temperature using a potentiostat (Interface 1000E, Gamry Instruments or Maccor 4300) from 4.25 to 3 V. The OCV of NMC111 vs. Li was measured using the Galvanostatic Intermittent Titration Technique (GITT, Supplementary Fig. 5). The coin cells were discharged at a constant current corresponding to a C-rate of C/10 in steps of 10% depth-of-discharge, followed by a pause at open circuit for 5 h to allow the voltage to relax prior to OCV measurement. This pulse/relaxation cycle was repeated until the 3 V cut-off voltage was reached.
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5

Surface-Modified Polymer Fiber Electrodes

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2 cm long fiber sections of surface-modified and unmodified with similar cross-sectional size (25.7 μm × 16.6 μm) were prepared and connected with copper wire via silver paint. A potentiostat (Interface 1000E, Gamry Instruments) was utilized to obtain the impedance measurement results with 1x phosphate-buffered saline (PBS, Thermo Fisher) as the electrolyte. To evaluate the change in impedance results before and after surface modification of the polymer electrode, we performed a three-electrode experiment with polymer fiber, Ag/AgCl electrode (Cole-Pamer), and a Pt wire (Basi), which serve as working electrode, reference electrode, and counter electrode respectively. An AC voltage of 10 mV with frequency ranging from 10 Hz to 100 kHz was applied, and the impedance measurement results were recorded accordingly. In order to discover the impact of silver oxidation on electrode electrical characteristics, the polymer fiber tip was soaked in 1X PBS, and two-electrode EIS experiments were conducted daily for two weeks, which mimic the two-electrode recording environment in mouse brain. The exciting AC voltage remained the same, while the frequency range changed to 100 Hz to 10 kHz.
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6

Characterization of Lithium-ion Battery Materials

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The powder X-ray diffraction (XRD) patterns were collected using a Rigaku D/max-2500 with Cu Ka radiation. Atomic force microscope (AFM) images were obtained with a Digital Instruments nanoscope IIIa (Multimode, Veeco), operating in tapping mode. Fourier transform infrared (FTIR) spectra were recorded using a FTIR spectrometer (VERTEX 70v spectrometer, Bruker) in the wave number range of 400–4,000 cm−1. Scanning electronic microscopy (SEM) images were performed using a Hitachi SU8020 electron microscopy.
The cells were assembled in an argon-filled glove box. The half-cells were charged and discharged with a constant current between 2.5 V and 4.0 V. The charge/discharge cycling studies were performed on a battery test system (LAND CT2001, China). Electrochemical impedance spectra tests (EIS) were carried out in the frequency ranging from 0.1 to 100 KHz in an electrochemical workstation (Autolab). Linear sweep voltammetry (LSV) was conducted in an electrochemical workstation (Interface-1000E, Gamry) using Li/composite/stainless steel cells and the sweeping voltage ranged from 2.6 to 6.0 V with a scanning rate of 10 mV s−1.
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7

Electrochemical DNA Biosensor Calibration

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To establish a baseline against which to compare, each sensor was first examined by EIS (Gamry Interface 1000E). A dilution series of strands of the target DNA segment (Integrated DNA Technologies, Inc., USA) in PBS solution was prepared, yielding 10 µM, 8 µM, 6 µM, 4 µM and 3 µM solutions. For each concentration, 2 sensors were then each exposed to 100 µL of analyte solution for 30 min. Following exposure, the sensors were rinsed with a small amount of ethanol to remove unbound target DNA before being submerged in a PBS solution for testing. The tests were performed in a 3-electrode configuration using a standard testing cell (Fig. S11, supplied by Gamry Instruments Inc) connected to the potentiometer via common banana connector cables. All EIS measurements herein were carried out according to the parameters in Table S8.
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8

Electrochemical and Mechanical Characterization of Hydrogels

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Potentiostatic electrochemical impedance spectroscopy was conducted between f=10−2 Hz to 106 Hz with an amplitude of 20 mV (Interface 1000e, Gamry Instruments, Warminster, PA) while the hydrogel strain was controlled using a custom machined micromanipulator. Cyclic voltammetry was conducted with the same instrument at −3 to 3 V and −1 to 1 V using an Ag/AgCl reference electrode, a platinum counter electrode, and a gold-coated custom flexible PCB working electrode at scan rates between 40–500 mV/s at 21.4 oC. Mechanical properties of hydrogels were measured using uniaxial stress-strain measurements (Instron 5943 with Bluehill Software, Instron, Norwood, MA) at 21.4 oC and 43% relative humidity. Electromechanical properties with the hydrogel on the Instron were measured at 10 kHz with an amplitude of 20 mV and a sampling rate of 10 Hz (ADG5940, Analog Devices, Wilmington, MA). DC resistance measurements were conducted using a 10 μA input current (Keithley 2400, Tektronix Inc., Beaverton, OR).
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9

Electrochemical Characterization of MoO3 Anode

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Cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS) measurements were conducted on a Gamry (Interface 1000 E Potentiostat) electrochemical workstation. The galvanostatic discharge and charge profiles were measured by the NEWARE-CT-4008 battery tester. The working electrodes were prepared by mixing the MoO3, super conductive carbon black (SCCB, Ketjenblack EC-600JD, Lion Corporation, Tokyo, Japan) and polyvinylidene fluorid (PVDF) binder in N-methyl-2-pyrrolidone (NMP) with a weight ratio of 8:1:1. After stirring for 1 h, the homogeneous slurry was coated onto a copper foil. The mass loading of the active material was estimated to be about 1.0 mg cm−2. The CR2032 coin-type cells using the fabricated product were assembled in an argon-filled glovebox (oxygen/moisture concentrations < 0.01 ppm). Celgard 2400 porous polypropylene membrane was used as the separator. The electrolyte is 1 M LiPF6 in carbonate (EC)/dimethyl carbonate (DMC) with the volume ratio of 1:1.
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10

Electrochemical PEDOT:PSS Microarray Fabrication

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First, Au-pl and Au-nr macro-/microarrays were fabricated following a similar procedure to that of spin-coated PEDOT:PSS devices up to PEDOT:PSS coating step. At the final step, PEDOT:PSS film was electrodeposited rather spun-cast. Prior to the PEDOT:PSS electrodeposition, 20 CV cycles were performed on all channels within −0.6–0.6 V versus Ag/AgCl in PBS as an electrochemical cleaning step. Then PEDOT:PSS was electrodeposited from 0.01 M EDOT in 2.0 g per 100 mL NaPSS aqueous dispersion (both were purchased from Sigma-Aldrich) under potentiostatic conditions at a potential of 0.9 V versus Ag/AgCl in a three electrode setup, i.e., Ag/AgCl electrode as a reference electrode, a large platinum electrode as a counter electrode, and the target microarray/macrodot arrays as the working electrode, at a constant temperature of 27 °C using a GAMRY interface 1000E. Polymerization was driven for 20 s at or below current density of 0.5 mA cm−2, resulting in ≈220 nm thick PEDOT:PSS film deposition on the electrode sites.
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