The morphologies and sizes of mCaCO3 and sCaCO3 were observed on scanning electron microscopes (Apero/Nova NanoSEM, FEI) and on a transmission electron microscope (Tecnai TF20, FEI). The composition was detected by Fourier transform infrared spectroscopy (Nexus 670, Thermo-Nicolet), Raman spectroscopy (Renishaw inVia Raman Microscope), X-ray diffraction (Ultima IV, Rigaku). The content of water was measured by thermogravimetric analysis (TGA) using a thermogravimetric analyzer (Q200, TA).
Nanosem
The NanoSEM is a scanning electron microscope (SEM) designed for high-resolution imaging of nanoscale materials and structures. It utilizes a focused electron beam to scan the surface of a sample, producing detailed images that reveal the topography and composition of the specimen at the nanometer scale. The NanoSEM is capable of visualizing a wide range of materials, including metals, semiconductors, and biological samples, making it a valuable tool for research and development in fields such as materials science, nanotechnology, and life sciences.
Lab products found in correlation
7 protocols using nanosem
Synthesis and Characterization of Modified and Spherical Calcium Carbonate
The morphologies and sizes of mCaCO3 and sCaCO3 were observed on scanning electron microscopes (Apero/Nova NanoSEM, FEI) and on a transmission electron microscope (Tecnai TF20, FEI). The composition was detected by Fourier transform infrared spectroscopy (Nexus 670, Thermo-Nicolet), Raman spectroscopy (Renishaw inVia Raman Microscope), X-ray diffraction (Ultima IV, Rigaku). The content of water was measured by thermogravimetric analysis (TGA) using a thermogravimetric analyzer (Q200, TA).
Oxide Nanoflake Device Fabrication
Nanofiber Mesh Platinum Sputter Coating
Electron Microscopy Sample Preparation
High-Resolution Scanning Electron Microscopy
Optical and Structural Characterization of Oligomer Nanoparticles
nanoparticles and silver-decorated
oligomer nanoparticles were characterized by a UV–vis spectrophotometer
(Carry, UV–vis) and a florescence spectrophotometer (Carry
Eclipse Florescent Spectrophotometer). The morphologies of oligomer
and silver nanoparticle were investigated using focused ion beam scanning
electron microscopy (FEI, NanoSEM) and transmission electron microscopy
(FEI Technai G2 F30). Determination of the size distribution and average
diameter of nanoparticles with respect to their hydrodynamic sizes
were carried out via dynamic light scattering (DLS) measurements (Malvern
Nano-ZS Zetasizer). Chemical and elemental analysis of nanoparticles
were determined using X-ray photoelectron spectroscopy (XPS) (Thermo
Fisher Scientific). Measurements were performed with a spot size of
∼400 μm, 30 eV pass energy, and 0.1 eV step size. The
powder X-ray diffraction system (X’pert pro MPD (PANalytical))
to study the XRD patterns of the hybrid materials.
All chemicals
and solvents were purchased from Sigma Aldrich Chemical
Co. (Germany), including silver nitrate salt. Detailed synthesis and
characterization of the oligomer were reported in our previous publications.30 (link),33 (link)
Synthesis and Characterization of SnSe Nanoparticles
After that, the furnace was cooled down to room temperature naturally. Angle-resolved conductivity measurement: The SnSe NPs from mica substrate were transferred to a 300 nm SiO 2 /Si substrate, where pre-patterned markers had been defined. [22] Then, PMMA (ethyl lactate, 950 kMW) of about 280 nm in thickness was spun on the substrate and baked at 170° for 5 min. Later, the star-shaped 12 electrodes (220 nm Au) were defined on a SnSe NP by electron-beam lithography (FEI NanoSEM), followed by development, thermal evaporation and lift-off processes. All electrical characterizations were performed using a Keithley 4200 semiconductor parameter analyzer.
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