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Benzyl ether

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Benzyl ether is a chemical compound used as a solvent and intermediate in various organic synthesis reactions. It is a colorless liquid with a characteristic odor. Benzyl ether has a molecular formula of C6H5CH2OCH2C6H5 and a molar mass of 198.26 g/mol.

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Lab products found in correlation

Oleic acid, by Thermo Fisher Scientific (3 mentions) Iron acetylacetonate, by Thermo Fisher Scientific (2 mentions) Oleylamine, by Merck Group (2 mentions) Tetraethyl orthosilicate, by Thermo Fisher Scientific (2 mentions) Zinc acetylacetonate, by Thermo Fisher Scientific (2 mentions) Octadecene, by Merck Group (1 mentions) Cadmium chloride, by Thermo Fisher Scientific (1 mentions) Zinc chloride, by Thermo Fisher Scientific (1 mentions) Cobalt 2 chloride, by Merck Group (1 mentions) Di tert butyl disulfide, by Merck Group (1 mentions) Copper 2 chloride, by Merck Group (1 mentions) Lf from bovine colostrum, by Merck Group (1 mentions) Chloroform, by Sinopharm (1 mentions) Phenyl ether, by Thermo Fisher Scientific (1 mentions) Hexane, by Tokyo Chemical Industry (1 mentions) Ethylene glycol, by Tokyo Chemical Industry (1 mentions) Absolute ethanol, by Thermo Fisher Scientific (1 mentions) Dulbecco s phosphate buffered saline dpbs, by Merck Group (1 mentions) 3 4 5 dimethylthiazol 2 yl 2 5 diphenyltetrazolium bromide mtt, by Merck Group (1 mentions) Nickel acetylacetonate, by Merck Group (1 mentions)

8 protocols using benzyl ether

1

Synthesis of Colloidal Nanocrystals

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Copper(II) chloride [CuCl2, 97%], cobalt(II) chloride [CoCl2, 97%], octadecene [ODE,
90%, technical grade], and di-tert-butyl disulfide
[DTBDS, 97%] were purchased from Sigma-Aldrich. Zinc chloride [ZnCl2, 99.95%] and cadmium chloride [CdCl2, 99.99%]
were purchased from Alfa Aesar. Benzyl ether [BE, 99%] was purchased
from Acros Organics. Trioctylphosphine [TOP, >85%] was purchased
from
TCI America. All solvents (hexanes, isopropyl alcohol [IPA], acetone,
and toluene) were of analytical grade. All of the above chemicals
were used as received without further purification. Distilled oleylamine
[d-OLAM] was obtained via vacuum
distillation of oleylamine [t-OLAM, 70%, technical
grade, Sigma-Aldrich].24 (link)
O’Boyle S.K., Fagan A.M., Steimle B.C, & Schaak R.E. (2022). Expanded Tunability of Intraparticle Frameworks in Spherical Heterostructured Nanoparticles through Substoichiometric Partial Cation Exchange. ACS Materials Au, 2(6), 690-698.
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2

Luminescent Theranostic Nanoparticle Synthesis

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Iron (III) acetylacetonate (Fe(acac)3), oleylamine, and benzyl ether were purchased from Acros Organics (Geel, Belgium). Lf from bovine colostrum and fluorescent aminoluciferin were purchased from Sigma-Aldrich (St. Louis, MO, USA). Poly(vinyl alcohol) (PVA-217, 1700 of polymerization degree, 88.5 % of hydrolysis degree) was obtained from Kuraray (Tokyo, Japan). Chloroform was purchased from Sinopharm (Shanghai, China). α-Malemidyl-ω-N-hydroxysuccinimidylpoly(ethylene glycol) (NHS-PEG-MAL, MW3400) was obtained from Jenkem Technology (Beijing, China). Male Wistar rats (250–300 g) were supplied by Hubei Center for Disease Control and Prevention (Animal Qualification Certificate No. 4200060003926). All other reagents were of analytical grade.
Luo B., Wang S., Rao R., Liu X., Xu H., Wu Y., Yang X, & Liu W. (2016). Conjugation Magnetic PAEEP-PLLA Nanoparticles with Lactoferrin as a Specific Targeting MRI Contrast Agent for Detection of Brain Glioma in Rats. Nanoscale Research Letters, 11, 227.
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3

Synthesis and Characterization of Magnetic Nanoparticles

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Iron acetylacetonate (Fe(acac)3), cobalt acetylacetonate (Co(acac)2), phenyl ether, benzyl ether, oleic acid (OA), and absolute ethanol were obtained from (ACROS ORGANIC, Morris Plains, NJ, USA), Tungsten hexachloride (WCl6) and 1-octadecene were purchased from (Alfa Aesar Inc., Haverhill, MA, USA), Oleylamine (OAm), hexane, ethylene glycol, 3-(3,4-dihydroxy)hydrocinnamic acid (DHCA), tetrahydrofuran (THF), NaOH, and phosphate buffered saline (PBS, concentration of PO42− ions (0.0067 M) were acquired from Tokyo Chemical Industry (TCI Co, Tokyo, Japan), (Fisher chemicals, Pittsburgh, PA, USA), (J.T.Baker, Phillipsburg, NJ, USA), (Sigma Aldrich, St. Louis, MO, USA) (ECHO CHEMICAL CO., LTD., Taipei, Taiwan), (SHOWA Chemical, Tokyo, Japan), and HyCloneTM, Marlborough, MA, USA) respectively. The above chemicals were used without further purification. The 3-[4,5-dimethylthiazol-2yl]-2,5-diphenyl tetrazolium bromide (MTT) and Dulbecco’s Phosphate Buffered Saline (DPBS) were purchased from (Sigma Aldrich, St. Louis, MO, USA).
Hatamie S., Shih P.J., Chen B.W., Wang I.J., Young T.H, & Yao D.J. (2020). Synergic Effect of Novel WS2 Carriers Holding Spherical Cobalt Ferrite @cubic Fe3O4 (WS2/s-CoFe2O4@c-Fe3O4) Nanocomposites in Magnetic Resonance Imaging and Photothermal Therapy for Ocular Treatments and Investigation of Corneal Endothelial Cell Migration. Nanomaterials, 10(12), 2555.
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4

Colloidal Synthesis of Metal Nanoparticles

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Nickel acetylacetonate (Ni(acac)2, 95%), oleylamine (OAm, 70%), tributylphosphine (TBP, 97%), and ammonia molybdate ((NH4)6Mo7O24·4H2O) were purchased from Sigma-Aldrich and used without any further purification. Benzyl ether (BE, 99%) was bought from Acros Organics and used without any further purification. Isopropanol and hexane were purchased from Fisher (ACS Certified), distilled before use and kept with molecular sieve. All experiment was conducted under standard Schlenk line condition.
Lin L., Liu J., Liu X., Gao Z., Rui N., Yao S., Zhang F., Wang M., Liu C., Han L., Yang F., Zhang S., Wen X.D., Senanayake S.D., Wu Y., Li X., Rodriguez J.A, & Ma D. (2021). Reversing sintering effect of Ni particles on γ-Mo2N via strong metal support interaction. Nature Communications, 12, 6978.
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5

Synthesis and Characterization of Iron Oxide Nanoparticles

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All chemicals were purchased at reagent grade or better from the Sigma-Aldrich company (St. Louis, MO), unless otherwise noted. Iron (III) oxide nanopowder, less than 50 nm in size, was examined for hyperthermia applications, primarily as a low-cost, abundant nanomaterial. fluidMAG D with starch coating, and fluidMAG PAD with polyacrylamide coating were purchased from chemicell GmbH (Berlin, Germany), with a reported concentration of 100 mg/mL (which included the weight of the polymer coating). Both fluidMAG particles had a reported hydrodynamic radius of 50 nm. Additional iron oxide NPs dispersed in hexane were synthesized as described below, using iron(III) acetylacetonate 97%, 1,2-hexadecanediol 90%, oleic acid 90%, oleylamine 70% (Sigma-Aldrich, St. Louis, MO), benzyl ether 99% (Acros Organics, Fair Lawn, NJ), hexane, and ethyl alcohol. Table 1 lists the types, abbreviations, sizes, and concentrations of particles used for this study. alginic acid, sodium salt (Acros Organics, rated at 485 mPa-s for a 1% solution at 20 °C) was used to modify the viscosity of aqueous NP dispersions. Calcium chloride was purchased from Fisher Scientific (Fair Lawn, NJ) to cross-link alginic acid solutions.
Shah R.R., Davis T.P., Glover A.L., Nikles D.E, & Brazel C.S. (2015). Impact of magnetic field parameters and iron oxide nanoparticle properties on heat generation for use in magnetic hyperthermia. Journal of magnetism and magnetic materials, 387, 96-106.
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6

Synthesis of Multifunctional Nanoparticles

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Iron acetylacetonate (Fe(acac)3, 99%), zinc acetyl-acetonate (Zn(acac)2, 95%), benzyl ether (99%), tetraethyl orthosilicate (TEOS, 95%), dimercaptosuccinic acid (DMSA, 99%) and poly(sodium-p-styrene sulfonate) (PSS, linear, Mw ~70,000 g/mol) were purchased from Acros organics (USA). Polyethyleneimine (PEI, branched, Mw ~25,000 g/mol) and citric acid (CA, 99%) were received from Sigma-Aldrich (USA). Polyallylamine hydrochloride (PAAm, linear, 120,000<Mw<200,000 g/mol), oleic acid (90%) and ammonium hydroxide (NH4OH, 30%) were purchased from Alfa Aesar (USA). Ethanol (EtOH, 200 proof) was acquired from Decon Lab (USA). Dimethyl sulfoxide (DMSO, 99%) and toluene (99%) were obtained from Fisher Scientific (USA). All chemicals were used as-received without further purification.
Park J., Porter M.D, & Granger M.C. (2015). Silica Encapsulation of Ferrimagnetic Zinc Ferrite Nanocubes Enabled by Layer-by-layer Polyelectrolyte Deposition. Langmuir : the ACS journal of surfaces and colloids, 31(11), 3537-3545.
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7

Synthesis of Colloidal Nanostructures

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Benzyl ether (C12H10O, 98%), oleic acid (C18H34O2, 90%) and cobalt acetylacetonate (Co(acac)2) were purchased from Alfa Aesar. Oleylamine (C18H37N, 50%) was acquired from TCI. 1-Octadecene (C18H36, 90%) and zinc acetylacetonate (Zn(acac)2) were bought from Acros Organics. 1,2-Decanediol was obtained from Aldrich. All the chemical regents in the experimental process were used as received without further purification.
Zong Y., Sun Y., Meng S., Wang Y., Xing H., Li X, & Zheng X. (2019). Doping effect and oxygen defects boost room temperature ferromagnetism of Co-doped ZnO nanoparticles: experimental and theoretical studies. RSC Advances, 9(40), 23012-23020.
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8

Synthesis of 64Cu-Incorporated Iron Oxide Nanoparticles

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To synthesize 64Cu-incorporated iron oxide (64Cu-IO) NPs, we purchased the reagents acetylacetone, sodium acetate, copper chloride, benzyl ether, iron acetylacetonate, lauric acid, dodecylamine, cyclohexane, ammonia hydroxide, and tetraethylorthosilicate from Alfa Aesar. In addition, reagents 1,2-hexadicanediol and igepal CO-520 were purchased from Sigma Aldrich (Burlington, MA, USA). 64Cu was supplied by Korea Institute of Radiological & Medical Sciences.
Jang H.M., Jung M.H., Lee J.S., Lee J.S., Lim I.C., Im H., Kim S.W., Kang S.A., Cho W.J, & Park J.K. (2022). Chelator-Free Copper-64-Incorporated Iron Oxide Nanoparticles for PET/MR Imaging: Improved Radiocopper Stability and Cell Viability. Nanomaterials, 12(16), 2791.
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