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Fls 980 apparatus

Manufactured by Edinburgh Instruments

The FLS 980 is a high-performance fluorescence spectrometer designed for advanced photoluminescence and time-resolved fluorescence measurements. It features dual monochromators, a high-sensitivity detector, and a wide range of accessories to accommodate various sample types and experimental requirements. The FLS 980 is a versatile instrument suitable for a broad range of applications in materials science, life sciences, and analytical chemistry.

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2 protocols using fls 980 apparatus

1

Nanomaterial Characterization Protocol

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UV-Vis absorption spectra were measured by using a TU-1901 dual beam UV-Vis spectrophotometer. Transmission electron microscopy (TEM) micrographs were obtained using a FEI Tecnai G2 S-twin transmission electron microscope. The sample for the X-ray diffraction (XRD) assay was obtained by depositing the product solution on glass slides and vacuum drying at 80 °C. Fourier-transform infrared (FT-IR) spectra were recorded on a Vertex Perkin-Elmer 580BIR spectrophotometer (Bruker). Up conversion emission spectra were recorded on an Edinburgh FLS 980 apparatus, from 400 to 700 nm, using a 980 nm laser diode module as the irradiation source. The N2 adsorption–desorption isotherm and pore-size distribution were observed on a Micromeritics Tristar 3000 instrument.
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2

Structural and Optical Characterization of Novel Materials

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A sample for X-ray diffraction (XRD) analysis was prepared by depositing the sample solution on glass slides and vacuum drying at 80 °C. The XRD patterns of the samples were recorded on a D8 Focus diffractometer (Bruker) using CuKa radiation (λ = 0.15405 nm). Transmission electron microscopy (TEM) micrographs were obtained using a FEI Tecnai G2 S-twin transmission electron microscope with a field emission gun operating at 200 kV. Fourier-transform infrared (FT-IR) spectra were obtained on a Vertex Perkin-Elmer 580BIR spectrophotometer (Bruker), using the KBr pellet technique. The N2 adsorption–desorption isotherm and pore-size distribution were tested on a Micromeritics Tristar 3000 instrument. UV-vis absorption spectra were acquired using a TU-1901 dual beam UV-vis spectrophotometer. Upconversion emission spectra were measured on an Edinburgh FLS 980 apparatus, from 400 to 700 nm, using an 808 nm laser diode module as an irradiation source.
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