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Cdcl3

Manufactured by Fujifilm

CDCl3 is a laboratory solvent commonly used in nuclear magnetic resonance (NMR) spectroscopy. It is a clear, colorless liquid with a characteristic chloroform-like odor. CDCl3 is widely employed as a solvent for the analysis of organic compounds due to its excellent solvent properties and compatibility with NMR instrumentation.

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2 protocols using cdcl3

1

Synthesis and Characterization of Acrylate Compounds

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Methyl acrylate (1), ethyl acrylate (2), n-butyl acrylate (3), and methyl methacrylate (4) were purchased from Toagosei Co., Ltd. γ-Cyclodextrin (γCD) was obtained from Junsei Chemical Co. Ltd. 1-Hydroxy cyclohexyl phenyl ketone (Ciba, IRGACURE 184) was purchased from BASF Japan Co., Ltd. 2-Ethyl-2-adamantyl acrylate (Ad) was obtained from Osaka Organic Chemical Industry Ltd. 1,4-Butanediol diacrylate (BDA), acetic anhydride, and bromoethane were purchased from Nacalai Tesque Inc. Lithium bis(trifluoromethanesulfonyl)imide (LiTFSI) was purchased from Tokyo Chemical Industry Co., Ltd. PAcγCD was prepared according to Scheme S1 in ESI (Fig. S1–S3). EMIm TFSI was prepared according to Scheme S2 and S3 in ESI (Fig. S4–S8). Pyridine and CDCl3 were purchased from Wako Pure Chemical Industries, Ltd. DMSO–d6 was obtained from Merck & Co., Inc. Water used for the preparation of the aqueous solutions was purified with a Millipore Elix 5 system. Other reagents were used without further purification.
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2

Synthesis of Photosensitive Acrylamide Polymers

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N,N-Dimethylacrylamide (DMAA) and CDCl3 were purchased from FUJIFILM Wako Pure Chemical Corporation. N,N-Diethylacrylamide (DEAA) and 4-acrylloylmorpholine (ACMO) were purchased from KJ Chemicals Corporation. Ammonium peroxodisulfate (APS) and 2,2’-azobis(isobutyronitrile) (AIBN) were purchased from Nacalai Tesque Inc. Deuterium oxide (D2O) was purchased from Sigma–Aldrich (Louis, MO, USA). The water used for the preparation of the aqueous solutions was purified with a Milli-Q ® Integral MT system. Other reagents were used without further purification. Azobenzene acrylamide (AzoAAm) was prepared according to a previous report [51 (link)].
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