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2 protocols using nah2po4 2h2o

1

Synthesis and Modification of Layered Double Hydroxides

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The following materials were used for synthesis and anion modification of LDHs: Al(NO3)3·9H2O (98.5%, Chempur), Mg(NO3)2·6H2O (99%, Chempur), NaCl (99.9% Chempur), NaH2PO4·2H2O (>98% Carl Roth), Na2HPO4·2H2O (>98% Scharlau), HNO3 (66%, REACHEM s.r.o.), C2H6O2 (99%, Sigma-Aldrich), HCl (36%, Chempur). Deionised and decarbonised water was used for syntheses, preparation of solutions and washing of final products.
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2

Synthesis and Characterization of Redox-Active Compounds

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Na2HPO4.2 H2O, NaH2PO4.2 H2O, NaCl and potassium ferricyanide were purchased from Carl Roth; potassium ferrocyanide, neutral red (NR) from Sigma. All chemicals had higher purity than 98% and were used without further purification. Humic acid (20 wt% ash) and lignin (alkali) were from Aldrich.
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