Tungsten 6 chloride

Manufactured by Merck Group

Tungsten(VI) chloride is a chemical compound with the formula WCl6. It is a crystalline solid that is commonly used as a precursor in the synthesis of other tungsten compounds and materials. Tungsten(VI) chloride has a high boiling point and is generally stable under normal conditions.

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2 protocols using tungsten 6 chloride

Synthesis and Characterization of Tungsten Complexes

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All materials were handled in an inert
atmosphere (Ar) glovebox or using standard Schlenk techniques (N₂). All reaction solvents were dried and deoxygenated using
an Innovative Technology PS-MD-4 solvent purification system and stored
over activated 3 Å molecular sieves. DMEDA (98%), DEEDA (95%),
and tungsten(VI) chloride (99.9%) were purchased from Sigma-Aldrich
and purified. WCl₄(DME) (DME = dimethoxyethane) was synthesized
using a previously reported procedure in the literature.^{26 (link)} The ¹H and ¹³C NMR spectra
were recorded using a Bruker Advance NEO 500 MHz FT-NMR spectrometer.
All samples for the NMR spectra were sealed in an NMR tube containing
C₆D₆ as internal standards inside the Ar atmosphere
glovebox. The Fourier-transform infrared (FT-IR) spectra were obtained
using a Shimadzu IRSpirit FT-IR spectrophotometer. Samples were prepared
within the glovebox using pellets with KBr. Elemental analysis was
performed using a Thermo Scientific FLASH EA-2000 organic elemental
analyzer.

Son J.Y., Kim S.H., Seo J.M., Lim J., Chung T.M, & Park B.K. (2023). Synthesis and Characterization of Tungsten Amide Complexes for the Deposition of Tungsten Disulfide Thin Films. ACS Omega, 8(22), 19816-19821.

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Synthesis and Characterization of Nanoparticles

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Gadolinium(III) acetate hydrate (99.9% trace metals basis), ytterbium(III) chloride hexahydrate (99.9%), tantalum(V) chloride (99.8%), tungsten(VI) chloride (99.9%), gold(III) chloride trihydrate (99.9%), bismuth(III) nitrate pentahydrate (98.0%), tantalum(V) ethoxide (99.98%), cyclohexane (99%), IGEPAL CO-520, ammonium hydroxide solution (28.0–30.0% NH₃ basis) and calcium phosphate (96.0%) were purchased from Sigma-Aldrich (St. Louis, MO). 2-(carbomethoxy)ethyltrimethoxysilane and 3-(trimethoxysilyl)propyl-N,N,N-trimethylammonium chloride were obtained from Gelest, Inc (Morrisville, PA). Iomeron 400 mg/ml was purchased from Bracco (Milan, Italy). The cell lines used for in vitro experiments, HepG2, Renca, SVEC4-10EHR1, were provided by ATCC (Manassas, VA). LIVE/DEAD assay kits were purchased from Life Technologies Invitrogen (Grand Island, NY).

Kim J., Bar-Ness D., Si-Mohamed S., Coulon P., Blevis I., Douek P, & Cormode D.P. (2018). Assessment of candidate elements for development of spectral photon-counting CT specific contrast agents. Scientific Reports, 8, 12119.

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