The largest database of trusted experimental protocols

2 protocols using methoxyperfluorobutane

1

Synthesis and Characterization of Functional Materials

Check if the same lab product or an alternative is used in the 5 most similar protocols
The following chemicals were used as received: sodium dodecyl sulphate (≥99%), Sudan Red 7B (95%), 1,6-hexanediol diacrylate (80%), 1,4-butanediol diacrylate (90%), trimethylolpropane ethoxylate triacrylate (Mn = 428 g mol−1), 1,2-dichlorobenzene (99%), Zonyl FS-300 (40% solids), methoxyperfluorobutane (99%), mineral oil (light), iron(II) chloride tetrahydrate (99.99%), 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol (97%), methacrylic acid (99%) and octadecane (99%) (Sigma-Aldrich); silicone oil (for oil baths −40 to +200 °C), perfluorohexanes (98%), hexanes (98%), and iron(III) chloride (98%) (Alfa Aesar); ethyl nonafluorobutyl ether (>98%) and sodium oleate (>97%) (TCI); Darocur 1173 (Ciba); fluorinated acrylate oligomer (Sartomer); Nile Red (99%) (Acros); N-dodecylpropane-1,3-diamine (>95%) (Matrix). Light-responsive surfactant was made by the literature procedure26 ,32 . Fluorinated coumarin dye was made by the literature procedure31 (link). Cleavable surfactant sodium 2,2-bis(hexyloxy)propyl sulphate was made by the literature procedure28 (link).
+ Open protocol
+ Expand
2

Photoluminescent Polymer Optical Fiber

Check if the same lab product or an alternative is used in the 5 most similar protocols
Several thermoplastic polymers are suitable and commercially available [39 ,40 (link)] for a PL-POF core. We have chosen the cycloolefin (COP) polymer, which was previously identified as the best host material for a specific photoluminescent dye, Lumogen Red 305 (LR305), as the formation of dye aggregates is less pronounced in this material [15 (link)]. COP granulates (Zeonor 1020R, refractive index 1.53) were purchased from Zeon Europe GmbH, Düsseldorf, Germany. The photoluminescent dye, LR305 (BASF, Basel, Switzerland), was added to the COP core at a concentration of 0.01 wt.%. The terpolymer of tetrafluoroethylene, hexafluoropropylene and vinylidene fluoride polymer (THVP), has become a common choice for the sheath material of melt-processed POFs [12 (link),15 (link),29 (link),31 (link)]. THVP is characterized by good transparency, low RI, good melt-spinnability, and semi-crystallinity [41 (link)]. THVP granulates (THVP 2030GZ, RI = 1.35) were purchased from 3M GmbH, Rüschlikon, Switzerland. Acetone and methoxyperfluorobutane were purchased from Sigma Aldrich, Buchs, Switzerland, in order to remove the sheath for subsequent studies of the optical and structural properties of the core material. All materials were used as provided without purification.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!