Analysis of nicotine by potentiometric titration was carried out using a TruLab pH 1310P (YSI Incorporated, Xylem Inc, USA) potentiometric pH meter with TruLine 15 glass electrode selective to H+ ions and containing silver chloride reference electrode. Liquid-Liquid Extraction was carried out using a Waters Alliance 2695 quaternary pump HPLC equipped with Waters 996 PDA Detector, Hypersil Gold Phenyl column (150 mm × 4.6 mm, 3 μm, Thermo Scientific™, USA), and a Security Guard Cartridge Phenyl (4 mm × 2.0 mm, Phenomenex, USA). Waters Empower 2 software was used for processing data. NMR analysis was carried out using Bruker NanoBay AVANCE III 400 MHz NMR spectrometer (Bruker Corporation, USA).
Nanobay avance 3 400 mhz nmr spectrometer
Manufactured by Bruker
Sourced in United States
The NanoBay AVANCE III 400 MHz NMR spectrometer is a compact and versatile nuclear magnetic resonance (NMR) instrument designed for high-resolution analysis. It features a 400 MHz superconducting magnet and advanced electronics to enable precise measurements of molecular structures and dynamics.
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2 protocols using nanobay avance 3 400 mhz nmr spectrometer
1
Quantification of Nicotine by Potentiometric Titration
2
Nanomaterial Characterization by NMR
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This journal is © The Royal Society of Chemistry 2020
Nanoscale, 2020, with hexane by centrifugation. The solid products were kept under vacuum for further characterization studies. NMR analysis was performed by mixing ∼50 mg of the solid to 750 µl of CDCl 3 . 1 H NMR spectra were recorded using a Bruker NanoBay AVANCE III 400 MHz NMR spectrometer.
Nanoscale, 2020, with hexane by centrifugation. The solid products were kept under vacuum for further characterization studies. NMR analysis was performed by mixing ∼50 mg of the solid to 750 µl of CDCl 3 . 1 H NMR spectra were recorded using a Bruker NanoBay AVANCE III 400 MHz NMR spectrometer.
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