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6 protocols using potassium chloride (kcl)

1

Synthesis of Ceramic Precursors

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Titanium dioxide (TiO2), iron oxide (Fe2O3), and magnesium carbonate basic pentahydrate (4MgCO3·Mg(OH)2·5H2O) were purchased from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). Potassium carbonate (K2CO3), sodium carbonate (Na2CO3), sodium chloride (NaCl), and potassium chloride (KCl) were purchased from Shanghai Lingfeng Chemical Reagent Co., Ltd., China. Ilmenite (FeTiO3) was purchased from Jiangsu Taibai Group Co., Ltd. (Zhenjiang, China). The alumina crucibles (50 mL) used for calcination were purchased from Nanjing Wanqing Chemical Glass Instrument Co., Ltd. (Nanjing, China).
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2

Synthesis of Bismuth Nanostructures

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Bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) and absolute ethanol (C2H5OH) were provided by Sinopharm Chemical Reagent Co., Ltd., Shanghai, China. Selenium powder, sodium molybdate dihydrate (Na2MoO4·2H2O), and sodium borohydride (NaBH4) were purchased from Shanghai Adamas Reagent Co., Ltd., Shanghai, China. Potassium chloride (KCl) was obtained from Shanghai Lingfeng Chemical Reagent Co., Ltd., Shanghai, China. All the reagents were analytically pure grade and used as received without further purification. Milli-Q water was homemade and the resistivity was 18.2 MΩ cm.
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3

Deoxynivalenol Detection in Soil Samples

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All samples were collected between September and October 2021; the samples were transported at room temperature to the lab and stored at 4 °C before use. Three samples were taken from Linfen (Shanxi, China), including expJ from a chicken stable, expY from a sheep stable and expT from a wheat field. The sample expM was taken from a horse stable in Hangzhou (Zhejiang, China). ExpJ, expY and expM were materials of stable soil with animal waste and ExpT was the soil in the wheat field; the samples were collected with a grid soil-sampling method composed of four parallel transects [40 (link)] in closed bags with the aseptic technique.
Deoxynivalenol (≥99.9%), (Triple Chemical Corp. Ltd., Guelph, ON, Canada), Acetonitrile (>99.9%), (Anhui Tiandi High Purity Organic Solvent Co., Ltd., Anqing, China), high-performance liquid chromatography (HPLC), and a Waters e2695 and Waters 2998 photodiode array detector (Waters Shanghai Corp., Ltd., Shanghai, China) were used.
Culture medium: NaHCO3 0.06 g/L (Sinopharm Group Chemical Reagent Co., Ltd., Shanghai, China), KCl 0.01 g/L (Shanghai Lingfeng Chemical Reagent Co., Ltd., Shanghai, China), MgSO4·7H2O 0.12 g/L (Sinopharm Group Chemical Reagent Co., Ltd.), and CaCl2 0.29 g/L (Chengdu Kelon Chemical Co., Ltd., Chengdu, China); pH 7.8 ± 0.2.
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4

Electrochemical Sensing with Ionic Liquids

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Pyrrole, ammonium persulfate, horseradish peroxidase (HRP, EC1.11.1.17, 190 unit·mg−1) were purchased from Tokyo Chemical Industry Co., Ltd. (Tokyo, Japan). 1-Ethyl-3-methylimidazolium bromide ([C2mim]Br, 99%), 1-hexyl-3-methylimidazolium bromide ([C6mim]Br, 99%), and 1-dodecyl-3-methylimidazolium bromide ([C12mim]Br, 99%) were provided by Monils Chem. Eng. Sci. & Tech. (Shanghai) Co. Ltd. (Shanghai, China). K4Fe[(CN)6], K3Fe[(CN)6], Na2HPO4, NaH2PO4, KCl, citric acid and 30% hydrogen peroxide (H2O2) solution were obtained from Shanghai Lingfeng Chemical Reagent Co., Ltd. (Shanghai, China). Hydrogen tetrachloroaurate hydrate (HAuCl4, Au 28.6%) was provided by Shanghai Macklin Biochemical Co. Ltd. (Shanghai, China). Ascorbic acid (AA), D-(+)-glucose and uric acid (UA) were obtained from Aladdin Industrial Co., Ltd. (Shanghai, China). Sodium deoxycholate (NaDC, 98%) and aspartic acid (Asp, 98%) were purchased from Shanghai J&K Scientific (Shanghai, China). Ultrapure water with a resistivity of 18.2 MΩ·cm from a Simplicity water purification system (Millipore, Boston, MA, USA) was used for preparing buffer solutions with different pHs. All other chemicals were of analytical reagent grade and used without further purification.
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5

Reagent Acquisition for Biochemical Assays

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GAB (CAS 60142-96-3, purity > 98%) was purchased from Aladdin Industrial Corporation. NaCl (CAS 7647-14-5, purity > 99.5%) was purchased from Xilong Scientific Co., Ltd. CaCl2·2H2O (CAS 10035-04-8, purity > 99.0%) was purchased from Sinopharm Chemical Reagent Co., Ltd. MgSO4·7H2O (CAS 10034-99-8, purity > 99.0%), NaHCO3 (CAS 144-55-8, purity > 99.5%) and KCl (CAS 7447-40-7, purity > 99.5%) were purchased from Shanghai Lingfeng Chemical Reagent Co., Ltd. The CAT kit (Cat. no: KGT017), the GSH kit (Cat. no: KGT006), the GST kit (Cat. no: KGT005), the LDH kit (Cat. no: KGT02448), the·OH kit (Cat. no: KGT010) and the Bradford protein quantitation assay kit (Cat. no: KGT801) were purchased from KeyGEN bio TECH Co., Ltd.
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6

Synthesis and Characterization of D201 Resin

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The D201 resin, styrene–diethylene benzene copolymer with quaternary ammonium group (mean diameter of 0.7–0.8 mm) was purchased from Hangzhou Zhengguang Technology, Co., Ltd. (Hangzhou, China). D201 was washed with 1.5 M NaOH, 1.5 M HCl, distilled water, and ethanol to remove the potential residual impurities and dried at 40 °C for 24 h before use. FeCl3·6H2O, MgCl2·6H2O, NaH2PO4·2H2O, Na2SiO3, and diphenylcarbazide were purchased from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China) K2Cr2O7, NaCl, CaCl2, Na2SO4, and NaOH were purchased from Xilong Science Co., Ltd. (Shantou, China). HCl, NaNO3, and NaHCO3 were purchased from Nanjing Chemical Reagent Co., Ltd. (Nanjing, China). KCl and KBH4 were purchased from Shanghai Lingfeng Chemical Reagent Co., Ltd. (Shanghai, China). Anhydrous ethanol was purchased from Shanghai Titan Scientific Co., Ltd. (Shanghai, China). All chemicals were of analytical grade and all solutions were prepared with ultrapure water.
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