Deuterated trifluoroacetic acid

Manufactured by Merck Group

Sourced in United States

Deuterated trifluoroacetic acid is a laboratory chemical compound used as a solvent and reagent in various analytical and synthetic applications. It is a clear, colorless liquid with a distinctive odor. The deuterated version of trifluoroacetic acid is commonly used in nuclear magnetic resonance (NMR) spectroscopy to facilitate the analysis of samples.

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Trifluoroacetic acid (1109 citations) Deuterated trifluoroacetic acid (TFA-d) (3 citations)

3 protocols using deuterated trifluoroacetic acid

Synthesis and Characterization of Camphor Derivatives

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1,7,7-Trimethylbicyclo[2.2.1]heptan-2-one (( ±)-Camphor, > 95%), DL-2,3-dihydroxybutanedioic acid (DL-tartaric acid, ≥ 99%), trimethyl orthoformate (99%), sulfuric acid (95–98%), sodium bicarbonate (NaHCO₃, 99.0%), ethylene glycol (EG, 1,2-ethanediol ≥ 99.8%), 1,4-butanediol (99%), 1,6-hexanediol (99%), dimethyl terephthalate (99%), titanium(iv) isopropoxide, (99.995%) and chloroform-d (99.8 atom % D), and deuterated trifluoroacetic acid were purchased from Sigma-Aldrich. ( ±)-Camphor was recrystallized from ethanol.

Kang J.H., Sim S.J., Lee J.H., Lee S, & Suh D.H. (2022). Bio-Degradable Polyesters with Rigid Cyclic Diester from Camphor and Tartaric Acid. Journal of Polymers and the Environment, 30(8), 3463-3473.

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Synthesis of Ruthenium Complexes

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Potassium trifluoromethanesulfonate and 1,10-phenanthroline
monohydrate were acquired from Sigma-Aldrich (Merk, Spain) and ruthenium
trichloride trihydrate (RuCl₃·3H₂O) from
Johnson Matthey. Deuterated solvents were obtained from Eurisotop,
except for deuterated trifluoroacetic acid, which was obtained from
Sigma-Aldrich. All chemicals were used as received without further
purification.

Ballester F.J., Hernández-García A., Santana M.D., Bautista D., Ashoo P., Ortega-Forte E., Barone G, & Ruiz J. (2024). Photoactivatable Ruthenium Complexes Containing Minimal Straining Benzothiazolyl-1,2,3-triazole Chelators for Cancer Treatment. Inorganic Chemistry, 63(14), 6202-6216.

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Myeloperoxidase Detection Protocol

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Sodium hypochlorite solution, acetonitrile, ethanol, formic acid, acetone (HPLC grade), methanol (MS grade), H₂O₂, NaCl, myeloperoxidase from human leukocytes (MPO), deuterated trifluoroacetic acid and D₂O were obtained from Sigma Chemical Co. (St. Louis, MO, USA).

Kumorkiewicz-Jamro A., Starzak K., Sutor K., Nemzer B., Pietrzkowski Z., Popenda Ł, & Wybraniec S. (2020). Structural Study on Hypochlorous Acid-Mediated Chlorination of Betanin and Its Decarboxylated Derivatives from an Anti-Inflammatory Beta vulgaris L. Extract. Molecules, 25(2), 378.

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