Mo kα

Manufactured by Rigaku

Sourced in Japan

The Mo Kα is an X-ray source that generates molybdenum Kα radiation. It is a core component of various analytical instruments used in scientific laboratories.

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Lab products found in correlation

Saturn 724 ccd diffractometer, by Rigaku (1 mentions) Saturn724 detector, by Rigaku (1 mentions) Afc12 goniometer, by Rigaku (1 mentions)

2 protocols using mo kα

X-ray Analysis of Compound 5

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Orange-red block crystals of 5 were obtained from a MeOH solution subjected to slow evaporation in a refrigerator for ca. 3 weeks. Single-crystal X-ray diffraction data were collected by a Rigaku Saturn 724 CCD diffractometer equipped with a multilayer-monochromator and a Mo Kα radiation (λ = 0.71073 Å) (Rigaku Co. Ltd., Japan). The structure was processed by direct methods, followed by Fourier techniques, and refined by SHELXL-97.²³ The block crystals of 5 are monoclinic, space group p2(1)/c with cell dimensions a = 7.6992(15) Å, b = 7.9904(16) Å, c = 24.276(5) Å, V = 1489.3(5) Å³, Z = 4, F (000) = 664, and goodness of fit on F² = 1.051. The R₁ and wR₂ values were 0.0644 [I > 2σ(I)] and 0.1361 (all data), respectively. Crystallographic data for compound 5 has been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 1497011. Copies of the data can be obtained, free of charge, on application to the CCDC, 12 Union Road, Cambridge CB2 1EZ, U.K. (fax, + 44 (0)-1223-336033; e-mail, deposit@ccdc.cam.ac.uk).

Wang K.B., Li D.H., Bao Y., Cao F., Wang W.J., Lin C., Bin W., Bai J., Pei Y.H., Jing Y.K., Yang D., Li Z.L, & Hua H.M. (2017). Structurally Diverse Alkaloids from the Seeds of Peganum harmala. Journal of natural products, 80(2), 551-559.

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X-Ray Crystallographic Structure Analysis

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Diff raction data were collected at 100 K on Rigaku AFC12 goniometer equipped with an enhanced sensitivity (HG) Saturn 724+detector mounted at the window of an FR-E+Superbright MoKα (λ = 0.71075 Å) rotating anode genera-tor with HF Varimax optics. 33 X-ray data were recorded and integrated using Rigaku CrystalClear 34 software. Crystal struc-ture was solved by direct methods using SHELXS-2013 35 and charge flipping methods using SUPERFLIP 36 and refined on Fo 2 by full-matrix least squares refinement using SHELXL-2013/2014 package. All non-hydrogen atoms were refined with anisotropic displacement parameters. All hydro-gen atoms were added at calculated positions and refined using a riding model with isotropic displacement parameters based on the equivalent isotropic displacement parameter (Ueq) of the parent atom. Figures were created using the ORTEP3 software package. 37 CCDC depository numbers: 969748, 990428 and

Hallett AJ ., Placet E ., Prieux R ., McCafferty D ., Platts JA ., Lloyd D ., Isaacs M ., Hayes AJ ., Coles SJ ., Pitak MB ., Marchant S ., Marriott SN ., Allemann RK ., Dervisi A , & Fallis IA . (2018). Exploring the cellular uptake and localisation of phosphorescent rhenium fac-tricarbonyl metallosurfactants as a function of lipophilicity. Dalton transactions (Cambridge, England : 2003), 47(40).

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