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6 bromohexanoyl chloride

Manufactured by Merck Group
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6-bromohexanoyl chloride is a chemical compound used as a laboratory reagent. It is a colorless to pale yellow liquid. The primary function of this product is to serve as a synthetic intermediate in organic chemistry reactions.

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Lab products found in correlation

Trifluoroacetic acid, by Merck Group (2 mentions) Anhydrous 1 2 dichloroethane, by Merck Group (1 mentions) Aluminum chloride, by Merck Group (1 mentions) Chlorobenzene, by Merck Group (1 mentions) Copper 1 bromide, by Merck Group (1 mentions) Trimethylamine solution, by Merck Group (1 mentions) Triton x 100, by Merck Group (1 mentions) Sodium azide, by Merck Group (1 mentions) Calcein, by Merck Group (1 mentions) 3 3 dipropylthiadicarbocyanine iodide, by Merck Group (1 mentions) N phenyl 1 naphthylamine, by Merck Group (1 mentions) Fluorescamine, by Merck Group (1 mentions) Hydrobromic acid, by Merck Group (1 mentions) Triphosgene, by Merck Group (1 mentions) Methanesulfonic acid, by Merck Group (1 mentions) Citraconic anhydride, by Merck Group (1 mentions) N n dimethylformamide (dmf), by Merck Group (1 mentions) Styrene, by Merck Group (1 mentions) Alcl3, by Merck Group (1 mentions) 1 2 dichloroethane, by Merck Group (1 mentions)

5 protocols using 6 bromohexanoyl chloride

1

Brominated PPO Membrane Synthesis

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Poly(2,6-dimethyl-1,4-phenylene oxide) (PPO) was purchased from Asahi Kasei Corp (Tokyo, Japan). 6-bromohexanoyl chloride, aluminum chloride, 1,2-dichloroethane anhydrous, trimethyl ammonium solution (45 wt% in DI water) and N,N,N’N’-tetramethyl-1,6-hexanediamine (TMHDA) were obtained from Sigma Aldrich Korea (Yongin, Korea). Methyl alcohol (MeOH), N-methyl-2-pyrrolidone (NMP) and potassium hydroxide (KOH) were purchased from Daejung Chemical (Siheung, Korea). The polyethylene (PE) support was provided from W-SCOPE KOREA (Ochang, Korea).
Son T.Y., Kim T.H, & Nam S.Y. (2020). Crosslinked Pore-Filling Anion Exchange Membrane Using the Cylindrical Centrifugal Force for Anion Exchange Membrane Fuel Cell System. Polymers, 12(11), 2758.
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2

Synthesis of Tailored PPO/SEBS Membranes

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Asahi Kasei Co. (Tokyo, Japan) provided the poly (2,6-dimethyl-1,4-phenylene oxide) (PPO) (Mn = 34 000 g mol−1, Mw = 59,000 g mol−1). Kraton (Houston, TX, USA) was requested to provide Poly(styrene-b-ethylene-co-butylene-b-styrene) (SEBS, A1533H) with a 57% styrene content. Trimethylamine solution (~45 wt% in H2O), copper(I) bromide (CuBr(I), 98%), chlorobenzene (99.5%), 6-bromohexanoyl chloride (97%), aluminum chloride (AlCl3), and 3-dimethylamino-1-propyne (97%) were all purchased from Sigma–Aldrich (St. Louis, MO, USA). The following substances were bought from TCI (Tokyo, Japan): N-bromosuccinimide (NBS, 98%), sodium azide (NaN3, 99%), N,N,N′,N″,N″-pentamethyldiethylenetriamine (PMDTA, 99%), and dimethylamine (approx. 10% in THF). Alfa-Aesar (Haverhill, MA, USA) provided triethyl silane (98%) for purchase. Alternative commercial providers were used to obtain other chemicals that were not mentioned above. Throughout the investigation, deionized (DI) water was used for membrane treatment and property evaluations.
Choi J., Min K., Mo Y.H., Han S.B, & Kim T.H. (2023). Understanding the Effect of Triazole on Crosslinked PPO–SEBS-Based Anion Exchange Membranes for Water Electrolysis. Polymers, 15(7), 1736.
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3

Synthesis and Characterization of Functionalized Compounds

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Methanesulfonic acid (MSA, 99%), 6-bromohexanoyl chloride (97%), sodium azide (99.5%), dibenzocyclooctyne-amine (DBCO-NH 2 ), N ε -carbobenzoxy-L-lysine (CbzLys, 99%), triphosgene (98%), trifluoroacetic acid (99%), hydrobromic acid (33 wt% in acetic acid), citraconic anhydride (CA, 98%), 3-(4,5dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide (MTT, 98%), 3,3′-dipropylthiadicarbocyanine iodide (DiSC 3 (5), 98%), N-phenyl-1-naphthylamine (NPN, 98%), fluorescamine (98%), calcein, and Triton X-100 were purchased from Sigma-Aldrich Corp. (St Louis, MO).
Pranantyo D., Kang E.T, & Chan-Park M.B. (2021). Smart nanomicelles with bacterial infection-responsive disassembly for selective antimicrobial applications. Biomaterials science, 9(5).
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4

Synthesis of Benzene-Sulfonyl Compounds

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Benzenesulfonyl chloride (99%), styrene (99%), 2,2′-azobis(2-methylpropionitrile) (AIBN; 0.2 M in toluene), activated basic alumina, AlCl3 (99%), 6-bromohexanoyl chloride (97%), 3-bromopropionyl chloride (technical grade), trifluoroacetic acid (97%), triethylsilane (98%), 45 wt% trimethylamine in H2O, anhydrous toluene, 1,2-dichloroethane, N,N-dimethylformamide (DMF), and N-methyl-2-pyrrolidone (NMP for HPLC) were obtained from Aldrich and used without further purification. KOH was obtained from Daejung Chemicals Co.
Chae J.E., Lee S.Y., Yoo S.J., Kim J.Y., Jang J.H., Park H.Y., Park H.S., Seo B., Henkensmeier D., Song K.H, & Kim H.J. (2021). Polystyrene-Based Hydroxide-Ion-Conducting Ionomer: Binder Characteristics and Performance in Anion-Exchange Membrane Fuel Cells. Polymers, 13(5), 690.
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5

Synthesis and Characterization of Novel Compounds

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Lithocholic acid (95%, Aldrich), lithium aluminum hydride (95%, Aldrich), 2-bromoacetyl chloride (95%, Aldrich) and 6-bromohexanoyl chloride (97%, Aldrich) were used as received. N,N,N′,N′-tetramethyl-1,2-ethanediamine (99%, TCI) and N,N,N′,N′-tetramethyl-1,6-hexanediamine (99%, Aldrich) were distilled before use. Tetrahydrofuran (THF) and N, N-dimethylformamide (DMF) were dried over drying columns. Ampicillin was purchased from VWR as the pure form. All other reagents and solvents were from commercial resources and used as received unless otherwise mentioned. Spectrum Spectra/Por® 3 Dialysis Membranes with MWCO 3500 were purchased from VWR. All other reagents used for biological assays were purchased from Thermo Fisher Scientific or Sigma Aldrich and will be mentioned in the respective sections.
Ganewatta M.S., Rahman M.A., Mercado L., Shokfai T., Decho A.W., Reineke T.M, & Tang C. (2018). Facially amphiphilic polyionene biocidal polymers derived from lithocholic acid. Bioactive Materials, 3(2), 186-193.
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