The largest database of trusted experimental protocols

2 protocols using 2 bromo 1 phenyl ethanone

1

Synthesis of Substituted Phenyl Cyclohexenes

Check if the same lab product or an alternative is used in the 5 most similar protocols
Solvents (AR), including methanol, ethyl acetate, hexane, anisole, and dichloromethane (DCM), and the reagents, such as phenyl cyclohexene (>95%), anthraquinone, phenyl hydrazine, 2-bromo-1-phenyl ethanone, benzoic anhydride, BHT, TEMPO, methanesulfonic acid, and dodecane (>99%), were all purchased from Sigma-Aldrich. The reactant, 4-methoxy- substituted phenyl cyclohexene, in the reaction scope was prepared with the literature method, and other reactants were prepared with similar method (49 (link)).
+ Open protocol
+ Expand
2

Deuterated Solvents and Organohalogens Synthesis

Check if the same lab product or an alternative is used in the 5 most similar protocols
Deuterated chloroform (CDCl3, 99.8% with 0.5% tetramethylsilane-TMS), deuterated methanol (CD3OD, 99.9%), deuterated dimethylsulfoxide (DMSO-d6, 99.9%) and deuterated acetone (acetone-d6, 99.9%) were purchased from Sigma-Aldrich. Ethyl acetate and hexane were purchased from Synth. Sodium azide was purchased from Merck. The reagents 2-bromo-1-phenylethanone (98%), 2-bromo-1-(4-methoxyphenyl)ethanone (97%), 2-bromo-1-(4-chlorophenyl)ethanone (98%), 2-bromo-1-(4-bromophenyl)ethanone (98%), 2-bromo-1-(4-fluorinephenyl)ethanone (98%), 2-bromo-1-(3-fluorinephenyl)ethanone (98%), (+)-sodium L-ascorbate (98%) and ethinylestradiol (≥98%) were purchased from Sigma-Aldrich.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!