Amazonx spectrometer

Manufactured by Bruker

Sourced in Germany

The AmazonX spectrometer is a laboratory instrument designed for spectroscopic analysis. It is capable of measuring and recording the interaction between matter and electromagnetic radiation. The core function of the AmazonX spectrometer is to provide accurate and reliable data for scientific research and analytical applications.

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Lab products found in correlation

Spectrum 400, by PerkinElmer (1 mentions) Avance 400 spectrometer, by Bruker (1 mentions) Ultraflex 3 tof tof spectrometer, by Bruker (1 mentions) Avance 400, by Bruker (1 mentions) Avance 500, by Bruker (1 mentions)

Close spelling variants of this product

AmazonX mass spectrometer Bruker spectrometers

2 protocols using amazonx spectrometer

Spectroscopic Characterization of Synthesized Compounds

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All NMR experiments were performed on the Bruker Avance-400 spectrometer. Chemical shifts were reported relative to deuterated water as an internal standard. Attenuated total internal reflectance, FTIR spectra of all compounds have been recorded using Spectrum 400 (Perkin Elmer) 4000 to 400 cm⁻¹ range. Analysis of elements C, H and N have been recorded using a Perkin-Elmer 2400 CHN elemental analyzer. MS experiments (electrospray ionization) were carried out using a AmazonX spectrometer (Bruker Daltonics, Bremen, Germany). The ionization parameters were as follows: positive ion mode; capillary voltage 4.5 kV, drying gas of 10 L/min nitrogen at 300 °C. Mass analyzer scanned from 100 to 2800 u. Melting points were determined using the Boetius Block apparatus. Chemicals were purchased from Sigma-Aldrich.
Compounds 1, 2 were synthesized by the authors of [40 (link),41 (link)].

Yakimova L., Kunafina A., Nugmanova A., Padnya P., Voloshina A., Petrov K, & Stoikov I. (2022). Structure–Activity Relationship of the Thiacalix[4]arenes Family with Sulfobetaine Fragments: Self-Assembly and Cytotoxic Effect against Cancer Cell Lines. Molecules, 27(4), 1364.

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Solvent Purification and Characterization Protocols

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Reactions were carried out under ambient atmosphere. All solvents employed were purified and dried according to standard methods prior to use. All chemicals were purchased from commercial suppliers and used as received. NMR experiments were carried out with Bruker spectrometers AVANCE-400 and AVANCE-500. Chemical shifts are reported in the δ ( ppm) scale relative to the residual solvent signals for 1 H and 13 C, to external C 6 F 6 (-164.9 ppm) for 19 F NMR spectra. Multiplicities are reported as follows: singlet (s), doublet (d), triplet (t), quartet (q), quintet (quin), sextet (sext), multiplet (m), broad resonance (br); coupling constants in Hz; integration. Mass spectra MALDI were recorded on a UltraFlex III TOF/TOF spectrometer (Bruker Daltonik GmbH, Germany) in a linear negative mode with a solution of molecular sulfur in toluene as a matrix using a metallic target. Laser Nd:YAG, λ = 266 nm. FlexAnalysis 3.0 program (Bruker Daltonik GmbH, Germany) was used to process the data. Mass spectra ESI were recorded on a AmazonX spectrometer (Bruker Daltonik GmbH, Germany) in negative and positive mode with capillary voltage -4500 V. The drying gas was nitrogen of 250 °C and flow of 8 l min -1 . Samples of 10 -6 g ml -1 concentration in THF or CH 3 CN were used for analysis.

Dudkina Y.B., Kholin K.V., Gryaznova T.V., Islamov D.R., Kataeva O.N., Rizvanov I.K., Levitskaya A.I., Fominykh O.D., Balakina M.Y., Sinyashin O.G, & Budnikova Y.H. (2016). Redox trends in cyclometalated palladium(ii) complexes. Dalton transactions (Cambridge, England : 2003), 46(1).

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