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Poremaster gt 60

Manufactured by Anton Paar
Sourced in United States

The Poremaster GT-60 is a gas adsorption analyzer designed to determine the pore size distribution and specific surface area of solid materials. It employs the principle of gas adsorption and desorption to provide detailed information about the porous structure of a wide range of samples.

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3 protocols using poremaster gt 60

1

Vacuum Freeze Drying of Fried Samples

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The fried samples were immersed in petroleum ether for 10 min to remove the oil, and then dehydrated by a vacuum freeze dryer (Labconco, Kansas City, MO, USA). The conditions of vacuum freeze drying were that the cold trap temperature of −80°C and a pressure of 5 Pa. Pores with an equivalent diameters of 0.005–350 μm were determined by mercury intrusion porosimetry (MIP) (Poremaster GT-60, Quantachrome Instruments, Boynton Beach, FL, USA) according to the method of Zhang et al. (23 (link)).
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2

Physical Characterization of 3D-Printed Ti6Al4V Implants

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The physical parameters of the 3D-printed Ti6Al4V implants were determined using the following methods. The true density was measured using a helium gas pycnometer (AccuPyc 1330 Gas Pycnometer; Micromeritics Instruments, Norcross, GA, USA) [46 (link)]. The specific surface area was calculated using the Brunauer-Emmett-Teller method with krypton (the Kr-BET method), as reported elsewhere [47 (link)]. The porosity was analysed using a mercury porosimeter (PoreMasterGT 60, Quantachrome Instruments, Boynton Beach, FL, USA) [48 (link)], and the mechanical strength was determined using a mechanical testing system (Landmark, MTS Inc., Eden Prairie, MN, USA). Compression tests were performed at an initial strain rate of 10−3 s−1 at room temperature [49 (link)]. Samples were measured in triplicate.
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3

Pore Properties Analysis of Potato Slices

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Pore properties and pore size distribution of potato slices (U0F0, U1F0, and U2F0) and fried samples (U0F1, U1F1, and U2F1) were measured by MIP, and a mercury porosimeter (Poremaster GT-60, Quantachrome Instruments, U.S.A.) was used to determine the pore characteristics according to the methodology implemented by Zhang et al. [29] with small revision. Before analyzing pore characteristics, samples have to be dehydrated and deoiled. These samples were dehydrated using freeze-drying, and then deoiled using Soxhlet method. After draining oil and water, the samples (the weight about 5 g) were placed in the penetrometer. Firstly, the penetrometer assembly was loaded in the low-pressure port. Secondly, residual air of potato chips was evacuated and the initial mercury intrusion subsequently took place. Finally, the penetrometer was transferred into the high-pressure port. Pressure ranged from 0.006 MPa to 69.431 MPa. The generated data was output and performed with Porowin software.
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