UV–vis absorption spectra were recorded with a Varian Cary 300 double beam spectrometer. Luminescence spectra were measured for air-saturated and degassed diluted (c ≈ 5·10–5 M) solutions in ethanol with a Horiba Jobin Yvon Fluorolog 3 steady-state fluorescence spectrometer. For decay time measurements a PicoQuant LDH-P-C-375 pulsed diode laser (λexc = 372 nm, pulse width 100 ps) was applied as the excitation source. The emission signal was detected with a cooled photomultiplier attached to a FAST ComTec multichannel scalar card with a time resolution of 250 ps. Photoluminescence quantum yields PL were determined with a Hamamatsu C9920-02 system equipped with a Spectralon® integrating sphere.
Cary 300 double beam spectrometer
Manufactured by Agilent Technologies
The Cary 300 double beam spectrometer is a laboratory instrument designed for ultraviolet-visible (UV-Vis) spectroscopic analysis. It is equipped with a double beam optical system, which allows for the simultaneous measurement of a sample and a reference. The instrument is capable of performing a range of spectroscopic measurements, including absorbance, transmittance, and reflectance, across a wavelength range of 190 to 900 nanometers.
Automatically generated - may contain errors
Lab products found in correlation
2 protocols using cary 300 double beam spectrometer
1
Photophysical Characterization of Organic Compounds
2
Synthesis and Characterization of Oxygenated Compounds
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All reactions were carried out under an atmosphere of argon using standard Schlenk techniques. Chromatographic separations were carried out using silica gel 60 (Merck, 230-400 mesh ASTM). Dichloromethane was purified by distillation from CaH 2 prior to use and methanol was purified by distillation over magnesium. 2,3-Dimethyl-1,3-butadiene, m-chloroperoxybenzoic acid, 30% hydrogen peroxide and selenium dioxide were purchased from commercial suppliers and were used without further purification.
Instruments 1 H NMR (600 MHz) and 13 C{H} NMR (150 MHz) spectra were recorded with a Bruker Avance III 600 spectrometer operating at 298 K in the Fourier transform mode. Chemical shifts are reported in δ units ( ppm) using as residual CDCl 3 ( 1 H δ 7.26 ppm, 13 C δ 77.00 ppm) as the reference. Infrared spectra were recorded with a FTIR Nexus Nicolet apparatus. Mass spectra were recorded with a Varian 500-MS iT mass spectrometer (ESI) or with a Finnigan Mat95 mass spectrometer (EI). Microanalyses were determined by Analytical Services of the Polish Academy of the Sciences, Łódź. UV-Vis absorption spectra were recorded with a Varian Cary 300 double beam spectrometer.
Instruments 1 H NMR (600 MHz) and 13 C{H} NMR (150 MHz) spectra were recorded with a Bruker Avance III 600 spectrometer operating at 298 K in the Fourier transform mode. Chemical shifts are reported in δ units ( ppm) using as residual CDCl 3 ( 1 H δ 7.26 ppm, 13 C δ 77.00 ppm) as the reference. Infrared spectra were recorded with a FTIR Nexus Nicolet apparatus. Mass spectra were recorded with a Varian 500-MS iT mass spectrometer (ESI) or with a Finnigan Mat95 mass spectrometer (EI). Microanalyses were determined by Analytical Services of the Polish Academy of the Sciences, Łódź. UV-Vis absorption spectra were recorded with a Varian Cary 300 double beam spectrometer.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!