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Alpha a impedance analyzer

Manufactured by Novocontrol

The Alpha-A Impedance Analyzer is a high-performance instrument designed for the measurement and analysis of electrical impedance. It provides a wide frequency range and high-precision data acquisition, enabling accurate characterization of various materials and devices.

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2 protocols using alpha a impedance analyzer

1

Characterization of 1-MP Capacitor Cell

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1-MP was ground very fine by employing mortar and pestle under ambient conditions (RH = 45 ± 5%, T = 25 ± 5°C). The powder was loaded into a homemade capacitor cell consisting of Aluminum (∼ 35 μm) bottom and top contacts mounted on polycarbonate sheets with about 100 μm thickness (setup, including dimensions in Figure S25). Electrical connections were arranged on opposite sides of the capacitor to avoid high frequency coupling. After loading the cell, it was sandwiched between two rubber pieces and a hydrostatic pressure of about 175 ± 20 kPa was applied. Electrical characterization was carried out by employing a Novocontrol alpha-A Impedance Analyzer. Temperature sweeps were controlled employing a Peltier element which was connected to a PID temperature controller for temperature stabilization. Cell calibration was done by employing a polyimide sheet, vide infra.
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2

Structural and Optical Properties of Ag-Doped ZnO

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The structural properties of the prepared materials were recorded by X-ray diffractometer (Rigaku SmartLab SE) in the 2θ range of 20 0 -80 0 using Cu as a target (Cu K α =1.5406 Å) at 45 kV and 40 mA. The morphology of bare ZnO and Ag (concentration = 1, 3, 5 mol%) doped ZnO were observed by scanning electron microscope (SEM -ZEISS EVO18) and highresolution transmission electron microscopy (HRTEM, TEM -Thermo sher: Talos F200S G2). FTIR spectra were recorded on a ThermoFisher Scienti c iS50 spectrometer. The Raman spectra of prepared nanomaterials were analyzed by Raman spectrometer (NOST: HEDA-URSM4/5/7). The charge transport properties of Ag/ZnO nanocomposites were studied using Novocontrol Alpha-A impedance analyzer. The data of UV-visible spectra were analyzed through a UV-Vis NIR spectrophotometer (JASCO, V-670). The spectra of photoluminescence (PL) were provided by JASCO FP-8300 spectro uorometer.
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