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Optima 200 dv

Manufactured by PerkinElmer
Sourced in United States

The Optima 200 DV is a dual-view inductively coupled plasma optical emission spectrometer (ICP-OES) designed for multi-element analysis. It provides simultaneous measurement of multiple elements in a single run, offering efficient and accurate analysis of a wide range of sample types.

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2 protocols using optima 200 dv

1

Comprehensive Characterization of TiO2/Ag Composites

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X-ray powder diffraction (XRD, Rigaku-DMax 2400) with a 2θ scan configuration in the range 5-80° in reflection mode (Cu-Ka radiation) was used to characterize the TiO 2 /Ag composites. Scanning electron microscope (SEM, Quanta-450, operated at 20 kV), field emission scanning electron microscope (FESEM, NOVA NANOSEM 450, measured at 15 kV) and energy dispersive X-ray (EDX, Quanta-450 instrument) were operated to check the size and morphologies of samples. The X-ray photoelectron spectroscopy (XPS, ESCALAB250) was employed to study the surface atomic composition and chemical state. The adsorption-desorption isotherms of the composites was performed on An ASAP 2020 physical absorption apparatus. The optical density (OD) and photocatalytic properties were measured by a cell density meter (CO8000) and UV-vis diffuse reflectance spectroscope (UV-550). Fluorescent-Based cell wall/membrane integrity assay was carried out with fluorescence microscopy (OLYMPUS BX51). The fluorescence spectroscope was operated on FP-8300 Fluorescence Spectrometer. A xenon arc lamp (BL-GHX-IV, operated at 300 W) was used to provide simulated solar irradiation.
Inductively coupled plasma atomic emission spectrometer (ICP-AES, Optima 200 DV, made by Perkin Elmer Company) was adopted to measure the silver content.
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2

Mineral Analysis via ICP-OES

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The mineral content was analyzed using the method of Kang et al. [15 (link)]. Take 500 mg of sample in the vessel, mix 7 mL of HNO3 and 2 mL of H2O2, pre-treat using microwave (Titan MPS Microwave, PerkinElmer, Waltham, MA, USA) for 10 min, and then dilute to 3.4% concentration with tertiary distilled water. For the sample, the concentration of minerals was calculated by measuring the intensity of the ion beam using Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES, OPTIMA200 DV, PerkinElmer, Waltham, MA, USA). The analysis conditions are as follows: step 1 (temperature: 145 °C, pressure max: 70 min, ramp time: 5 min, hold time: 5 min, power: 60%), step 2 (temperature: 200 °C, pressure max: 80 min, ramp time: 5 min, hold time: 20 min, power: 90%), step 3 (temperature: 50 °C, pressure max: 80 min, ramp time: 1 min, hold time: 10 min, power: 0%). The standard products for quantification were multi-element calibration standards (ICP multi-element standard solution IV, Sigma–Aldrich Co., St. Louis, MO, USA), and the phosphorus, potassium, magnesium, calcium, and sodium were measured.
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