The largest database of trusted experimental protocols

Sta 449 f1 jupiter thermoanalyzer

Manufactured by Netzsch
Sourced in Germany

The Netzsch STA 449 F1 Jupiter is a thermoanalyzer that combines simultaneous thermal analysis (STA) techniques. It can perform thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) measurements on a single sample simultaneously.

Automatically generated - may contain errors

2 protocols using sta 449 f1 jupiter thermoanalyzer

1

Elemental Analysis and Thermal Decomposition

Check if the same lab product or an alternative is used in the 5 most similar protocols
The elemental analysis of C, H, and O was carried out using a Vario EL III CHNOS Elemental Analyzer (Elementar, Langenselbold, Germany). The Cu content was determined based on edta titration in the presence of 1-(2-pyridylazo)-2-naphtol as an indicator [32 ]. Analysis for the studied compound [determined/theoretical (%)]: C 48.9/49.8; H 6.0/6.1; O 27.1/26.5; Cu 16.9/17.6. The FT-IR spectra were recorded on a Jasco FT/IR 6200 spectrophotometer (JASCO, Easton, MD, USA), in the form of KBr pellets, in the spectral range 4000–400 cm−1, with resolution 1 cm−1. The thermal decompositions were carried out with a Netzsch STA 449 F1 Jupiter thermoanalyzer (Netzsch-Geratebau GmbH, Selb, Germany) coupled with a Netzsch Aeolos Quadro QMS 403 mass spectrometer (Netzsch-Geratebau GmbH, Selb, Germany). Samples were heated in Al2O3 crucibles, in the temperature range 35–1000 °C, with the heating rate 10 °C/min in synthetic air (80% N2, 20% O2).
+ Open protocol
+ Expand
2

Characterization of Novel Materials via Spectroscopic Techniques

Check if the same lab product or an alternative is used in the 5 most similar protocols
The FT-IR spectra were recorded on the Jasco FT/IR 6200 spectrophotometer (JASCO, Easton, MD, USA), in the form of KBr pellets, in the spectral range 4000–400 cm−1. The UV-Vis diffuse reflectance spectra were recorded on a Jasco V-660 spectrometer (Jasco, Easton, MD, USA), in the spectral range 190–800 nm, using spectralon [44 (link)] as a standard with 100% reflectance. The thermal decompositions were carried out with the Netzsch STA 449 F1 Jupiter thermoanalyzer (Netzsch-Geratebau GmbH, Selb, Germany) coupled with the Netzsch Aeolos Quadro QMS 403 mass spectrometer (Netzsch-Geratebau GmbH, Selb, Germany). Samples were heated in corundum crucibles, in the temperature range 35–1000 °C, with the heating rate of 10 °C/min in synthetic air (80% N2, 20% O2). The XRPD patterns were recorded in a reflection mode on the XPert PRO MPD diffractometer (Malvern Panalytical Ltd., Royston, UK) equipped with CuKα1 radiation, a Bragg–Brentano PW 3050/65 high-resolution goniometer, and PW 3011/20 proportional point detector.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!