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3 protocols using copper acetate monohydrate

1

Synthesis and Characterization of Metal-Organic Compounds

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Copper acetate monohydrate (C4H6CuO4·H2O), cobalt(iii) acetate tetrahydrate (C4H6CoO4·4H2O), potassium monopersulfate triple salt (42–46% KHSO5 basis), and adenine were purchased from Shanghai Macklin Biochemical Co., Ltd. Doxorubicin (DOX) and absolute ethanol were purchased from Aladdin Chemistry, Co. (Shanghai) and used as received. N,N-dimethylformamide (C3H7NO, DMF) was purchased from Sinopharm Chemical Reagent Co., Ltd. Aqueous solutions were prepared with deionized water. All other chemicals used in this work were of analytical grade, obtained from commercial suppliers, and used without further purification unless otherwise noted.
The powder X-ray diffractometry (XRD) patterns were obtained using a D8 advance X-ray diffractometer (Bruker Company, Germany). Fourier transform infra-red (FT-IR) spectra were obtained using a spectrum one FT-IR spectrophotometer (PerkinElmer, USA) at room temperature. Morphologies of the samples were observed on a JSM6510LV scanning electron microscope (SEM, JEOL, Japan). The elemental composition of the sample was analyzed using energy dispersive X-ray spectroscopy (EDX) and elemental mapping in a Super-XTM system.
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2

Synthesis of Copper Nanoparticles on Polyester Fabric

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Copper acetate monohydrate (C 4 H 6 CuO 4 •H 2 O), sodium citrate dehydrate (C 6 H 5 Na 3 O 7 •2H 2 O), polyvinylpyrrolidone (MW = 58,000), ethylene glycol, ascorbic acid, sodium hydroxide, anhydrous ethanol, deionized water (with electrical conductivity 18 MΩ•cm) were provided by Shanghai Macklin Biochemical Technology Co., Ltd. (Shanghai, China). The woven polyester fabrics were obtained from Suzhou Feijun Textile Co., Ltd. (Suzhou, China). Poly(butyl acrylate) (MW = 210,000) was purchased from Dayang Chem (Hangzhou) Co., Ltd. (Hangzhou, China). All the chemicals and solvents were analytical grade and were used as received without further purification.
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3

Synthesis of Copper-Antimony Thin Films

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Copper acetate monohydrate (C4H6CuO4·H2O, 99.95%), antimony acetate (C6H9O6Sb, 99.99%), thiourea (CH4N2S, 99%), glycol methyl ether (C3H8O2, 99.5%), and selenium powder were purchased from Macklin Inc. (Shanghai, China).
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