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2 methyltetrahydrofuran

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2-methyltetrahydrofuran is a cyclic ether compound used as an organic solvent. It has the molecular formula C₅H₁₀O.

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Lab products found in correlation

Absolute ethanol, by Carlo Erba (1 mentions) Chloroform, by Thermo Fisher Scientific (1 mentions) Ethyl acetate, by Merck Group (1 mentions) Toluene, by Merck Group (1 mentions) Dichloromethane, by Merck Group (1 mentions) Urea, by Merck Group (1 mentions) Indole, by Merck Group (1 mentions) Iron 3 nitrate nonahydrate, by Merck Group (1 mentions) 4 nitrobenzaldehyde, by Merck Group (1 mentions) Acetone, by Honeywell (1 mentions) Ethanol, by Honeywell (1 mentions) Acetonitrile, by Honeywell (1 mentions) Nickel 2 nitrate hexahydrate, by Merck Group (1 mentions) Manganese 2 nitrate hexahydrate, by Merck Group (1 mentions) Nitric acid, by Carlo Erba (1 mentions) Mercuryitc, by Oxford Instruments (1 mentions) Optistatcf2, by Oxford Instruments (1 mentions) Uv 3600 plus, by Shimadzu (1 mentions)

2 protocols using 2 methyltetrahydrofuran

1

Synthesis of BIM and Aerogel Catalysts

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Chemicals were purchased from the following providers and used without further purification. BIM synthesis: Indole (99+%, Aldrich, St. Louis, MO, USA); 4-Nitrobenzaldehyde (>99%, Aldrich); Dichloromethane (>99%, Aldrich); Acetone (>99.5%, Honeywell, Charlotte, NC, USA); Acetonitrile (>99.5%, puriss. p.a., ACS reagent, reag. Ph. Eur., Aldrich); Chloroform (99.8%, ACS, Alfa Aesar, Haverhill, MA, USA); Diethyl ether (RPE-For analysis-ACS, Carlo Erba Reagents, Cornaredo, Italy); Ethanol (96–97.2%, Honeywell); Ethyl Acetate (>99.7% Chromasolv, Sigma-Aldrich, St. Louis, MO, USA); 2-methyltetrahydrofuran (99%, Alfa Aesar); Toluene (>99.5% ACS Reagent, Sigma-Aldrich).
Aerogel catalyst synthesis: tetraethoxysilane ((Si(OC2H5)4, Aldrich 98%, TEOS); Urea ((NH2CONH2), Sigma-Aldrich (99.0–100.5%); Absolute Ethanol (CH3CH2OH, Carlo Erba); Nitric Acid (HNO3, Carlo Erba); Iron (III) nitrate nonahydrate (Fe(NO3)3·9H2O, Sigma-Aldrich 98%); Manganese (II) nitrate hexahydrate Mn(NO3)2·6H2O, Sigma-Aldrich, ≥98%); Nickel (II) nitrate hexahydrate Ni(NO3)2·6H2O, Sigma-Aldrich, ≥97%).
Melis N., Loche D., Thakkar S.V., Cutrufello M.G., Sini M.F., Sedda G., Pilia L., Frongia A, & Casula M.F. (2024). Magnetic Aerogels for Room-Temperature Catalytic Production of Bis(indolyl)methane Derivatives. Molecules, 29(10), 2223.
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2

Temperature-Dependent UV-Vis-NIR Spectroscopy

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The steady state absorption spectra were measured using a UV-vis-NIR absorption spectrometer (UV-3600 Plus, Shimadzu). The temperature dependent absorption spectra were obtained using a homemade system comprising the UV-3600Plus absorption spectrometer, a cryostat (OptistatCF2, Oxford Instruments), an electronic temperature controller (MercuryiTC, Oxford Instruments) and a vacuum pump. The temperature was adjusted between 295 K and 78 K, and the sample was dissolved in 2-methyltetrahydrofuran (99%, Alfa Aesar), which can form a clear glass at low temperatures.
Kong J., Kuang Z., Zhang W., Song Y., Yao G., Zhang C., Wang H., Luo Y, & Zhou M. (2024). Robust vibrational coherence protected by a core–shell structure in silver nanoclusters. Chemical Science, 15(18), 6906-6915.
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