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2 protocols using iron 3

1

Comprehensive Carotenoid and Vitamin Analysis

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Retinyl acetate, β-carotene, α-carotene, vitamin D3 (> 95% pure), deuterated vitamin D3, 4-phenyl-1,2,4-triazoline-3,5-dione (PTAD), phytic acid, DMACA, vanillin, iron III, pancreatin, ammonium thiocyanate, catechins, α-amylase, pepsin, bile, ferric chloride and sodium carbonate were purchased from Sigma Aldrich (Saint-Quentin-Fallavier, France). Lutein, lycopene, phytoene and phytofluene were purchased from Extrasynthèse (Genay, France). Soyasaponin I was generously supplied by Stéphane Georgé, CTCPA Avignon. Canned tomato pulp, red bell peppers and Isio4 oil (Lesieur, Asnières, France) were purchased from a local supermarket (Marseille, France). Methanol, acetonitrile, hexane, dichloromethane, methyl-tert-butylether, acetone, ethanol absolute anhydrous, sulfuric acid, hydrochloric acid, nitric acid, formic acid, hydrogen peroxide were purchased from CarloErba Reagents (Peypin, France).
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2

Magnetic Nanoparticle Synthesis Protocol

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Magnetic nanoparticles used in this study were synthesized in-house. Iron (III), Iron (II), and NaOH were purchased from Sigma Aldrich (St. Louis, MO, USA). Hydrazine (N2H4) was purchased from Alfa Aesar (Lancashire, UK). All the chemicals were used without any further modification. Double-distilled water was used with maintained heating and a regular N2 supply.
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