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1 acenaphthenol

Manufactured by Merck Group

1-acenaphthenol is a chemical compound used in various laboratory applications. It is a crystalline solid with a melting point of approximately 98-100°C. 1-acenaphthenol is commonly used as a chemical intermediate and in the synthesis of other organic compounds. However, a detailed and unbiased description of its core function without extrapolation on intended use cannot be provided concisely.

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2 protocols using 1 acenaphthenol

1

Synthesis and Characterization of 3-NBA and 3-ABA

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3-NBA and 3-ABA were synthesized as described previously.28 (link),29 (link) The purity and identity of these compounds were verified by UV spectroscopy, high-resolution mass spectrometry, and high-field 1H NMR spectroscopy. All other chemicals were of the highest grade commercially available, and all solvents were of HPLC grade. (S)-(+)-1,2,3,4-tetrahydro-1-naphthol (S-tetralol), flavin adenine dinucleotide (FAD), dithiothreitol (DTT), 1-acenaphthenol, dicoumarol (Dic), menadione, and D-glucose-6-phosphate (G6P) were purchased from Millipore-Sigma (St. Louis, MO). Glucose-6-phosphate dehydrogenase (G6PD) from Leuconostoc mesenteroides was purchased from Worthington Biochemical Corporation (Lakewood, NJ). 1-(2-Cyano-3,12,28-trioxooleana-1,9(11)-dien-28-yl)-1H-imidazole (CDDO-Im) was purchased from Tocris Bioscience (Bristol, U.K.) and R-sulforaphane (SFN) was purchased from LKT Laboratories (St. Paul, MN).
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2

Synthesis and Characterization of Nitro-Aromatic Compounds

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3-NBA, N-OH-3-ABA, and 3-ABA were synthesized as
described previously.31 (link),57 (link),58 (link) The synthesis of 3-NOBA was performed from 3-ABA
following the experimental protocol reported by Fifer et al. for the synthesis
of similar nitroso-PAHs.59 (link) The
purity and identity of these compounds were verified by UV spectroscopy, high
resolution mass spectrometry, and high-field 1 (link) H NMR spectroscopy. All other chemicals were of the
highest grade available, and all solvents were of HPLC grade.
(S)-(+)-1,2,3,4-Tetrahydro-1-naphthol
(S-tetralol), flavin adenine dinucleotide (FAD), dithiothreitol
(DTT), 1-acenaphthenol, dicoumarol (Dic), allopurinol, rotenone, and
D-glucose-6-phosphate (G6P) were purchased from Millipore-Sigma (St. Louis, MO).
Nicotinamide adenine dinucleotide (NAD+) and nicotinamide adenine
dinucleotide phosphate (NADP+) were purchased from Roche Diagnostics
(Indianapolis, IN). Glucose-6-phosphate dehydrogenase (G6PD) was purchased from
Worthington Biochemical Corporation (Lakewood, NJ). Androsterone was purchased
from Steraloids (Wilton, NH); 2,6-dichloroindophenol (DCPIP) and salicylic acid
were purchased from Acros Organics (Geel, Belgium). Flufenamic acid (FA),
ursodeoxycholate, and indomethacin were purchased from ICN Biomedicals, Inc.
(Aurora, Ohio).
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