The largest database of trusted experimental protocols

16 protocols using eu2o3

1

Synthesis of Advanced Emitting Agents

Check if the same lab product or an alternative is used in the 5 most similar protocols
3-Aminopropyl triethoxysilane
(APTES), polyvinyl pyrrolidone (PVP), tetraethylorthosilicate (TEOS),
and 3-glycidoxypropyltrimethoxysilane (GPTMS) were obtained from Sigma-Aldrich
(Egypt). Both the epoxy resin (SC-15A) and hardener (SC-15B) were
obtained from Chemicals for Modern Building International (Egypt).
The raw materials employed in the synthesis of AEAs include Eu2O3, Al2O3, Dy2O3, H3BO3, and SrCO3 which
were obtained from Merck (Egypt).
+ Open protocol
+ Expand
2

Synthesis of RSrCoFeO6 Perovskites

Check if the same lab product or an alternative is used in the 5 most similar protocols
The RSrCoFeO6 (R =
Sm, Eu) samples were prepared by using the solid-state
reaction process. First, the precursor oxides Sm2O3 (Alfa Aesar, 99.9% REO), Eu2O3 (Alfa
Aesar, 99.9% REO), SrCO3 (Merck), Co2O3 (Merck, >99%), and Fe2O3 (Merck, >99%)
were
mixed in the proper stoichiometric ratio. Afterward, we placed the
mixture together with 20 zirconia balls (∼5 mm diameter) in
a Retsch PM100 planetary ball mill at 450 rpm for 30 min (dry without
a medium). Finally, the powder was thermally treated for 12 h at 1100
°C in an air atmosphere, thus obtaining the final compounds.
+ Open protocol
+ Expand
3

Synthesis and Luminescent Properties of Eu-Doped BaSiO3 Phosphors

Check if the same lab product or an alternative is used in the 5 most similar protocols
A series of Ba0.98SiO3:0.02Eu, Ba0.96SiO3:0.02Eu, and 0.02R (R = Li, K, Na, La, and Y) phosphors were prepared using a conventional solid-state reaction. The BaCO3 (99+%), SiO2 (particle size 5~20 nm, 99.5%), Eu2O3 (99.99%), K2CO3 (99+%), Li2CO3 (99+%), Li2O (97%), Na2CO3 (99+%), LaCl3 (99.99%), and Y2O3 (99.99%), purchased from Merck, were used as a raw materials but SiO2 was used 20% more to obtain a single-phase BaSiO3 sample. The raw materials were thoroughly mixed in an agate mortar and subsequently fired in air at 1100 °C for 4 h to synthesize the Eu3+-doped BaSiO3. The BaSiO3:Eu2+ samples were prepared by sintering the BaSiO3:Eu3+ samples again under a reduction atmosphere (95% N2 + 5% H2) at 1200 °C for 6 h. The specific formulations of the studied samples are shown in Table 1.
The crystal phase of the obtained samples was identified using an X-ray diffractometer (X’Pert PRO MPD-3040, Malvern Panalytical, Malvern, UK, CuKα1, λ = 1.5406 Å) operating at 40 kV and 30 mA with a scan speed of 0.02°/sec. The photoluminescence excitation (PLE) and emission (PL) spectra were measured using a fluorescent spectrofluorometer (JASCO FP-8500, JASCO, Tokyo, Japan) equipped with an integrating sphere (ISF-834, JASCO, Tokyo, Japan). All measurements were performed at room temperature.
+ Open protocol
+ Expand
4

Standardization of Europium(III) Solution

Check if the same lab product or an alternative is used in the 5 most similar protocols
Eu 2 O 3 (Merck, purity > 99.99%) was dissolved in nitric acid which was evaporated to dryness and 0.1 M HNO 3 was added to the solid residue. The concentration of Eu(III) was standardized by complexometric titration with EDTA using xylenol orange as the indicator. The Eu(III) in nitric acid was evaporated to dryness and an FAH-water mixture (50 wt%) was added to obtain the desired Eu(III) concentration.
+ Open protocol
+ Expand
5

Synthesis and Characterization of RESA

Check if the same lab product or an alternative is used in the 5 most similar protocols
TPU (1.2 g
cm–3) was supplied from Sigma-Aldrich. All solvents
including N,N-dimethylformamide
(DMF, ≥99%) and tetrahydrofuran (THF, 99%) were supplied from
Sigma-Aldrich and used as received without further purification. The
starting materials employed in the synthesis of RESA, including Dy2O3, Al2O3, H3BO3, Eu2O3, and SrCO3, were
supplied from Aldrich.
+ Open protocol
+ Expand
6

Rare-Earth Doped Ceramic Synthesis

Check if the same lab product or an alternative is used in the 5 most similar protocols
SrCO3 (≥99.9%), SiO2 (≥99.995%), Si3N4 (≥99.9%), and Eu2O3 (≥99.99%) were purchased from Aldrich Corporation. BaCO3 (≥99.9%) was purchased from J.T. Baker Corporation. All of the initial chemicals were used without further purification. Aluminum oxide crucibles and cylindrical molybdenum crucibles (20 mm × 50 mm) were used in the sintering process of the samples.
+ Open protocol
+ Expand
7

Synthesis of Eu and Gd Co-doped Y2O3 Nanoprobes

Check if the same lab product or an alternative is used in the 5 most similar protocols
Analytical graded Y2O3 (99.99%), Eu2O3 (99.99%), Gd2O3 (99.99%), HNO3 (70.0%), and urea (99.0%–100.5%) were purchased from Sigma-Aldrich (St. Louis, MO, USA) and used as received. Spherical Y2O3 nanoprobes co-doped with Eu3+ and Gd3+ were fabricated using a urea homogeneous precipitation method using the reported protocols [8 (link),9 (link),10 (link),11 (link),12 (link)]. Briefly, a sealed beaker with a freshly prepared aqueous solution of rare-earth nitrates (0.0005 mol in 40 mL of H2O) was placed into an electrical furnace and heated to 90 °C for 1.5 h. The dried synthesized precipitates were then calcined in air at 800 °C for 1 h to produce the oxide NPs. In all cases, the Eu3+ doping concentration was kept constant at 1 mol %, whereas the Gd3+ concentration was varied from 0 to 10 mol %.
+ Open protocol
+ Expand
8

Synthesis of Eu1-xPrxBCO Perovskites

Check if the same lab product or an alternative is used in the 5 most similar protocols
Eu2O3, Pr2O3 (Sigma-Aldrich, St. Louis, MO, USA, 99.99% purity), CuO (Alfa-Aesar, Haverhill, MA, USA, 99.999% purity), and BaCO3 (POCH, Gliwice, Poland, 99.6% purity) were used to prepare the Eu1xPrxBCO samples. First, the materials were synthesized by a conventional solid-state reaction method by calcining the stoichiometric weighed substrates at 950 °C for 24 h. Then, the sinters were crushed, ground, and calcination was repeated. Next, sintered materials were ground again and pelletized under a uniaxial pressure of 800 MPa. Finally, the pellets were annealed in an oxygen flow of 20 L/h at 920 °C. After 33 h, the temperature was lowered to 400 °C and held for the next 33 h, as described [8 (link),9 (link),30 ].
+ Open protocol
+ Expand
9

Synthesis of Red-Emitting GdYGd:Eu3+ Phosphor

Check if the same lab product or an alternative is used in the 5 most similar protocols
The red-emitting GdYGd:Eu3+ phosphor was obtained by applying a simple sol–gel method using the initial materials, including Y2O3 (Sigma-Aldrich 99.99%), Eu2O3 (Sigma-Aldrich 99.99%), Gd2O3 (Sigma-Aldrich 99.99%), H3BO3 (Sigma-Aldrich 99.99%), C6H8O7·H2O (Sigma-Aldrich 99.99%) and HNO3 (Merck, 67%). First, Y2O3, Eu2O3, and Gd2O3 oxides were magnetically stirred at room temperature in an HNO3 solution for 60 minutes to dissolve completely. During this process, H3BO3 and C6H8O7·H2O solutions were gradually dropped to obtain a transparent solution. Then, this solution was continuously stirred at 120 °C for 6 h to obtain a wet gel product. The wet gel was also stirred at 200 °C for 5 h to obtain a dry gel. The dry gel was ground using an agate mortar for 30 minutes in the next step. Finally, the received product was annealed at 600–1200 °C in the air for 5 h to achieve the final GdYGd:Eu3+ phosphor powders.
+ Open protocol
+ Expand
10

Rare Earth Oxide Characterization

Check if the same lab product or an alternative is used in the 5 most similar protocols
The materials utilized in this research were distilled water, acetonitrile (Merck), samarium oxide (Sm2O3, 99.9%, Sigma Aldrich), dysprosium oxide (Dy2O3, 99.9%, Sigma Aldrich), europium oxide (Eu2O3, 99.9%, Sigma Aldrich), gadolinium oxide (Gd2O3 99.9%, Sigma Aldrich), and nitric acid 65% (Merck).
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!