Thermal gravimetric analysis (TGA) was carried out under a nitrogen atmosphere. The samples were heated to 900 °C at 10 °C min−1 and held for 30 min. Elemental analysis (C, H, N, B) was performed by Mikroanalytisches Laboratorium Kolbe (Oberhausen, Germany). UV-Vis absorption spectra were recorded using a Cary 60 UV/Vis spectrophotometer (Agilent Technologies, Mulgrave, Victoria, Australia). Fluorescence emission was measured using a QuantaMaster C-60/2000 spectrofluorometer (Photon Technology International, Lawrenceville, NJ, USA). The surface morphologies of particles were observed using a scanning electron microscope (SEM) (JSM-6700F, JEOL, Tokyo, Japan) and a transmission electron microscope (TEM) (JEM-1400 Plus). The hydrodynamic diameters of the nanoparticles were measured in water at 25 °C by dynamic light scattering (DLS) using a Zetasizer Nano ZS instrument (Malvern Instruments, Worcestershire, UK).
Quantamaster c 60 2000 spectrofluorometer
Manufactured by Horiba
Sourced in United States
The QuantaMaster C-60/2000 is a spectrofluorometer, a device used to measure the fluorescence properties of samples. It is capable of performing steady-state and time-resolved fluorescence measurements across a wide range of wavelengths.
Automatically generated - may contain errors
Lab products found in correlation
Zetasizer nano zs instrument, by Malvern Panalytical (2 mentions)
Cary 60 uv vis spectrophotometer, by Agilent Technologies (2 mentions)
Jem 1400plus, by JEOL (1 mentions)
Jsm 6700f, by JEOL (1 mentions)
B acs 60, by Bruker (1 mentions)
500 mhz avance iiiinstrument, by Bruker (1 mentions)
Vario el chns elemental analyzer, by Elementar (1 mentions)
Tgs 2 thermogravimetric analyzer, by PerkinElmer (1 mentions)
Ftir instrument, by PerkinElmer (1 mentions)
Tecnai spirit biotwin, by Thermo Fisher Scientific (1 mentions)
3 protocols using quantamaster c 60 2000 spectrofluorometer
1
Thermal, Optical, and Morphological Characterization of Nanomaterials
2
Characterization of Silica Particles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Attenuated total reflection (ATR)
infrared spectra were recorded using a Perkin-Elmer FTIR instrument
(Perkin-Elmer Instruments). The fluorescence emission was measured
using a QuantaMaster C-60/2000 spectrofluorometer (Photon Technology
International, Lawrenceville, NJ, USA). 1H and 13C NMR spectra were recorded on a superconducting magnet NMR spectroscopy
400 MHz (Bruker B-ACS60). Solid-state 11B MAS NMR experiments
were performed on a Bruker 500 MHz Avance III instrument in the Chemical
Biological Center, Umeå University. X-ray photoelectron spectroscopy
(XPS) analysis was carried out using a spectrometer with a Mg Kα (excitation 1253.6 eV) X-ray source. For fluorescence
microscopy imaging, samples were deposited on a glass slide and observed
under a Nikon Eclipse E400 epifluorescence microscope equipped with
a CCD camera. The conditions of measurement were: exposure time: 0.2
s, readout rate: 1 MHz at 16-bit, preamplifier gain: 5×, output
amplifier: conventional. Elemental analysis was carried out using
a Vario EL CHNS elemental analyzer (Elementar, Germany). The surface
morphologies of silica particles were observed with a scanning electron
microscope (SEM; JEOLJSM-T300). Thermal gravimetric analysis (TGA)
was performed in synthetic air using a TGS-2 thermogravimetric analyzer
(Perkin–Elmer, USA). The samples were heated from 40 to 700
°C at 10 °C/min and held for 30 min.
infrared spectra were recorded using a Perkin-Elmer FTIR instrument
(Perkin-Elmer Instruments). The fluorescence emission was measured
using a QuantaMaster C-60/2000 spectrofluorometer (Photon Technology
International, Lawrenceville, NJ, USA). 1H and 13C NMR spectra were recorded on a superconducting magnet NMR spectroscopy
400 MHz (Bruker B-ACS60). Solid-state 11B MAS NMR experiments
were performed on a Bruker 500 MHz Avance III instrument in the Chemical
Biological Center, Umeå University. X-ray photoelectron spectroscopy
(XPS) analysis was carried out using a spectrometer with a Mg Kα (excitation 1253.6 eV) X-ray source. For fluorescence
microscopy imaging, samples were deposited on a glass slide and observed
under a Nikon Eclipse E400 epifluorescence microscope equipped with
a CCD camera. The conditions of measurement were: exposure time: 0.2
s, readout rate: 1 MHz at 16-bit, preamplifier gain: 5×, output
amplifier: conventional. Elemental analysis was carried out using
a Vario EL CHNS elemental analyzer (Elementar, Germany). The surface
morphologies of silica particles were observed with a scanning electron
microscope (SEM; JEOLJSM-T300). Thermal gravimetric analysis (TGA)
was performed in synthetic air using a TGS-2 thermogravimetric analyzer
(Perkin–Elmer, USA). The samples were heated from 40 to 700
°C at 10 °C/min and held for 30 min.
3
Characterization of Silica Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Attenuated total reflection (ATR) infrared spectra were recorded at room temperature in the range of 4000-525 cm À1 with a resolution of 4 cm À1 and 16 scans using a Perkin-Elmer FT-IR instrument. Thermal gravimetric analysis (TGA) was performed in synthetic air. The samples were heated to 700 1C at 10 1C min À1 and held for 30 min. Elemental analysis (C, H, N) was carried out using an Elemental Analyser, Model 1108 (Carlo-Erba, Milan, Italy). Elemental analysis for Br and B content was performed by Mikroanalytisches Laboratorium Kolbe (Germany). UV-Vis absorption spectra were recorded using a Cary 60 UV/Vis spectrophotometer (Agilent Technologies). Fluorescence emission was measured using a QuantaMaster C-60/2000 spectrofluorometer (Photon Technology International, Lawrenceville, NJ).
The surface morphologies of silica particles were observed using a scanning electron microscope (Thermal Field Emission SEM LEO 1560, Zeiss, Oberkochen, Germany) and a transmission electron microscope (Tecnai Spirit BioTWIN, FEI Company, Oregon, USA). The hydrodynamic diameter of the nanoparticles was measured at 25 1C by dynamic light scattering using a Zetasizer Nano ZS instrument (Malvern Instruments, United Kingdom).
The surface morphologies of silica particles were observed using a scanning electron microscope (Thermal Field Emission SEM LEO 1560, Zeiss, Oberkochen, Germany) and a transmission electron microscope (Tecnai Spirit BioTWIN, FEI Company, Oregon, USA). The hydrodynamic diameter of the nanoparticles was measured at 25 1C by dynamic light scattering using a Zetasizer Nano ZS instrument (Malvern Instruments, United Kingdom).
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!