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Unity inova 500 mhz 1h spectrometer

Manufactured by Agilent Technologies
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The Unity INOVA 500 MHz (1H) spectrometer is a nuclear magnetic resonance (NMR) instrument designed for high-resolution spectroscopy. It operates at a proton frequency of 500 MHz and is capable of analyzing a variety of chemical samples to obtain detailed structural information.

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Unity Inova 500 MHz spectrometer Inova 500 MHz (1H) spectrometer Unity Inova 500 MHz UNITY INOVA 500 spectrometer Inova 500 MHz spectrometer Unity Inova 500 Unity Inova spectrometer Inova 500 MHz Unity 500 MHz Inova 500 spectrometer

2 protocols using unity inova 500 mhz 1h spectrometer

1

High-Resolution 59Co-NMR Spectroscopy

Check if the same lab product or an alternative is used in the 5 most similar protocols
Samples of all measured compounds were made as 0.7 mL volumes of 30 mM concentrations in protiated distilled water. Spectroscopic measurements were made at 118 MHz (59Co) using an Agilent Unity INOVA 500 MHz (1H) spectrometer at a field strength of 11.74 T with a 5mm BB NMR probe. Before any data collection, standard shims, deuterium locking, and probe tuning were made on 1 M sample of K3[Co(CN)6] in D2O, the 59Co-NMR reference standard. During 59Co-NMR experiments, data were collected in the absence of shimming and locking due to field stability of the instrument. Each sample was measured across a temperature range of 10–60 °C in 10 °C intervals. For each regulated temperature interval, samples were allowed to thermally equilibrate for 15 min before the probe was tuned for each pulse experiment.
Ozvat T.M., Johnson S.H., Rappé A.K, & Zadrozny J.M. (2020). Ligand Control of 59Co Nuclear Spin Relaxation Thermometry. Magnetochemistry (Basel, Switzerland), 6(4), 58.
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2

High-Resolution 59Co-NMR Spectroscopy

Check if the same lab product or an alternative is used in the 5 most similar protocols
Samples of all measured compounds were made as 0.7 mL volumes of 30 mM concentrations in protiated distilled water. Spectroscopic measurements were made at 118 MHz (59Co) using an Agilent Unity INOVA 500 MHz (1H) spectrometer at a field strength of 11.74 T with a 5mm BB NMR probe. Before any data collection, standard shims, deuterium locking, and probe tuning were made on 1 M sample of K3[Co(CN)6] in D2O, the 59Co-NMR reference standard. During 59Co-NMR experiments, data were collected in the absence of shimming and locking due to field stability of the instrument. Each sample was measured across a temperature range of 10–60 °C in 10 °C intervals. For each regulated temperature interval, samples were allowed to thermally equilibrate for 15 min before the probe was tuned for each pulse experiment.
Ozvat T.M., Johnson S.H., Rappé A.K, & Zadrozny J.M. (2020). Ligand Control of 59Co Nuclear Spin Relaxation Thermometry. Magnetochemistry (Basel, Switzerland), 6(4), 58.
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