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3 protocols using 1 propanol

1

Synthesis of Zeolite NaA and Organic Compounds

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Jiangsu Nine Heaven High-Tech
provides zeolite NaA (≥99.0%). KNO3 (≥99.0%),
ethyl acrylate (≥98.0%), ethanol (≥99.7%), and Hammett
indicator set are purchased from Sigma-Aldrich. 1-Propanol (≥99.0%)
was purchased from J&K. All chemicals were used without further
purification.
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2

Synthesis and Characterization of Organic Compounds

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2-propanol-d8 (99%), KBr (99.95%), (E)-benzalacetone, (E)-4-(furan-2-yl)but-3-en-2-one (98.0%), 1,3-diphenyl-propen-3-one (97%), 1-propenylbenzene (96%), 4-phenyl-1-butene were acquired from Shanghai Aladdin Biochemical Technology Co., Ltd. 2-methylimidazole (99%), 1-propanol (99.5%), (E)-3-(2-furanyl)-2-propenal (98%), cinnamyl alcohol (98%) were purchased from J&K Scientific Ltd. Methanol (99.7%), ethanol (99.7%), 2-propanol (99.8%), pyridine (99.5%), benzyl alcohol were acquired from Concord Technology (Tianjin) Co., Ltd. KSCN (99.5%), (E)-1-phenyl-1-butene (97%), triphenylmethane (99%), cinnamaldehyde (98%) were purchased from Shanghai Macklin Biochemical Co., Ltd. 1-butanol (99.5%), triphenylMethanol (99%),dodecane (99%), boric acid (99.5%), Zn(NO3)2·6H2O, propylbenzene (99%), allylbenzene (98%), chitosan (99%) were acquired from Beijing InnoChem Science & Technology Co., Ltd. Cinnamyl acetate (97%) was acquired from TCI (Shanghai) Development Co., Ltd. 3-phenyl-1-propanol (98%) was purchased from Adamas-Beta. 4-hydroxy-3-methoxycinnamaldehyde (97%) was acquired from Sigma-Aldrich. t-butanol was purchased from Alfa Aesar. Nitrogen (99.99%), argon (99.99%) and hydrogen (99.99%) were provided by Beijing Analytic Instrument Company. All reagents were directly used without further purification.
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3

Quantitative Analysis of Short-Chain Fatty Acids

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Acetic acid (Lot No. C0027517, ≥99.7%) and propionic acid (Lot No. A15J7L9136, ≥99.5%) were purchased from Dr. Ehrenstorfer (Augsburg, Germany). Butyric acid (Lot No. 755WP0-JS, ≥99.8%) and valeric acid (Lot No. FGN01-JLBK, ≥99.0%) were purchased from TCI Development Co., Ltd. (Shanghai, China). Hexanoic-6,6,6-d3 acid (Lot No. ZZS17102803, 99.0%) was purchased from Shanghai Zzbio Co., Ltd. (Shanghai, China). Sodium hydroxide (Lot No. 160928, ACS grade) was purchased from Xilong Scientific Co., Ltd (Beijing, China). 1-Propanol (Lot No. LP700111, HPLC grade) and pyridine (Lot No. LB30R04, HPLC grade) were purchased from J&K Scientific Ltd. (Beijing, China). Propyl chloroformate (Lot No. 11502046, HPLC grade) and hexane (Lot No. E1725082, HPLC grade) were purchased from Shanghai Aladdin Bio-Chem Technology Co., Ltd. (Shanghai, China).
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