Ybcl3

Manufactured by Merck Group

YbCl3 is a chemical compound composed of the rare earth metal ytterbium and chlorine. It is a solid, crystalline material commonly used in various laboratory applications.

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5 protocols using ybcl3

Multistep Solution-Processed Perovskite Films

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The perovskite film was fabricated by a multistep solution‐process. 1 m PbCl₂ (Sigma‐Aldrich) in DMSO containing YbCl₃ (Sigma‐Aldrich) at a stoichiometric range of 0–9.1 mol% was spin coated onto glass substrates (quartz for optical measurements and TCO for LED device) at 3000 rpm for 30 s. After being dried at 90 °C for 15 min, 0.07 m CsCl methanol solution was spin coated onto PbCl₂ film at 3000 rpm for 30 s and continuingly heated at 250 °C for 5 min. This process was repeated for five times to obtain the ideal perovskite films. The obtained perovskite films were rinsed with isopropanol and dried 250 °C again for 5 min. The Cs₄PbCl₆ phase was obtained when PbCl₂ film slowly reacted with CsCl solution by spin coating at 2000 rpm for 30 s.

Ishii A, & Miyasaka T. (2020). Sensitized Yb3+ Luminescence in CsPbCl3 Film for Highly Efficient Near‐Infrared Light‐Emitting Diodes. Advanced Science, 7(4), 1903142.

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Synthesis of Rare-Earth Chloride Compounds

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GdCl₃, TiCl₄, TeCl₄, EuCl₃, ErCl₃, YCl₃, YbCl₃, CeCl₄, MoCl₆, and TaCl₅ were obtained from Sigma-Aldrich. NaOH was obtained from Sinopharm Chemical Reagent Co. Deionized water used in all experiments was obtained from a Milli-Q water system.

Cheng L., Shen S., Jiang D., Jin Q., Ellison P.A., Ehlerding E.B., Goel S., Song G., Huang P., Barnhart T.E., Liu Z, & Cai W. (2017). Chelator-Free Labeling of Metal Oxide Nanostructures with Zirconium-89 for Positron Emission Tomography Imaging. ACS nano, 11(12), 12193-12201.

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Synthesis and Characterization of Rare-Earth Chlorides

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The following materials were used in this
study: CsCl (Sigma, 99.999%), PbCl₂ (Sigma, 99.999%, anhydrous),
LaCl₃ (Sigma, >99.99%, anhydrous), CeCl₃ (Sigma,
99.99%, anhydrous), PrCl₃ (Sigma, 99.99%, anhydrous), NdCl₃ (AlfaAesar, 99.9%, anhydrous), SmCl₃ (Sigma, 99.9%,
anhydrous), SmI₂ (Sigma, 99.9%, anhydrous), EuCl₃ (Sigma, 99.99%, anhydrous), EuI₂ (Sigma, 99.999%, anhydrous),
GdCl₃ (Sigma, 99.99%, anhydrous), TbCl₃ (Sigma,
99.99%, anhydrous), DyCl₃ (Sigma, 99.99%, anhydrous), HoCl₃ (Sigma, 99.9%, anhydrous), ErCl₃ (Sigma, 99.9%,
ultra dry), ErI₃ (abcr, 99.9%, anhydrous), TmCl₃ (Sigma, 99.9%, anhydrous), YbCl₃ (Sigma, 99.99%, anhydrous),
LuCl₃ (Sigma, 99.99%, anhydrous).

Kubicki D.J., Prochowicz D., Hofstetter A., Ummadisingu A, & Emsley L. (2024). Speciation of Lanthanide Metal Ion Dopants in Microcrystalline All-Inorganic Halide Perovskite CsPbCl3. Journal of the American Chemical Society, 146(14), 9554-9563.

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Synthesis of Halide-Based Solid Electrolytes

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The halide SEs were prepared by ball milling and subsequent solid-state reaction. Raw materials of LiCl (99.9%), InCl₃ (99.99%), ScCl₃ (99.99%,), YCl₃ (99.99%), YbCl₃ (99.99%), LuCl₃ (99.99%) and ZrCl₄ (99.9%) were used as starting materials from Sigma-Aldrich. The stoichiometric starting materials were weighed and ball milled at 350 rpm for 12 h sealed in a ZrO₂ jar using 18 ZrO₂ balls in an Ar-filled glovebox with p(H₂O)/p < 0.1 ppm, p(O₂)/p < 0.1 ppm. During ball milling, the jar was opened to make the samples homogenous at each 5 h in a glovebox. Then, the resulting mixture was sealed in quartz tubes and annealed at 260 °C for 12 h with a heating rate of 2 °C min⁻¹ and cooled naturally to room temperature. After that, the obtained material was directly stored in an Ar-filled glovebox to prevent any moisture exposition.

Wang Q., Zhou Y., Wang X., Guo H., Gong S., Yao Z., Wu F., Wang J., Ganapathy S., Bai X., Li B., Zhao C., Janek J, & Wagemaker M. (2024). Designing lithium halide solid electrolytes. Nature Communications, 15, 1050.

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Synthesis of Rare-Earth Nanoparticles

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YCl 3 $6H 2 O (99.9%), YbCl 3 $6H 2 O (99.9%), ErCl 3 $6H 2 O (99.9%), NaOH (98%), NH 4 F (98%), 1-octadecene (90%) and Oleylamine (OM) were purchased from Sigma-Aldrich. Fluoresceinyl cypridina luciferin analogue (FCLA) was purchased from Tokyo Kasel Kogyo Co. Tokyo, Japan. ABT737 was purchased from Selleck Chemicals (Houston, TX). All chemicals were used as received without further purification. 2, 9, 16, 23-tetracarboxylic Zinc phthalocyanine and poly (ethylene glycol)-poly (L-histidine) (PEG-PHis) diblock copolymer were synthesized according to the references. [24] .

Liu X., Fan Z., Zhang L., Jin Z., Yan D., Zhang Y., Li X., Tu L., Xue B., Chang Y., Zhang H, & Kong X. (2017). Bcl-2 inhibitor uploaded upconversion nanophotosensitizers to overcome the photodynamic therapy resistance of cancer through adjuvant intervention strategy. Biomaterials, 144.

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