The alkanethiols (butanethiol, octanethiol, and dodecanethiol) used to modify the surfaces of Ag/Cu powders were purchased from Sigma-Aldrich. Ag/Cu powder dispersed in isopropyl alcohol (IPA), without surface treatment after Ag coating, was supplied by JC Metal (Korea). The epoxy resin (YDPN 644, epoxy equivalent weight = 195–235 g/eq) and curing agent, phthalic anhydride (MNA), employed in the preparation of electrically conductive films were supplied by Kukdo Chemical (Korea). Toluene (99.5 %, Daejung Chemical, Korea) served as a diluent. All chemicals were used as received, without purification.
Butanethiol
Manufactured by Merck Group
Butanethiol is a colorless, flammable liquid with a strong, unpleasant odor. It is commonly used as a chemical intermediate in the production of other compounds.
Automatically generated - may contain errors
Lab products found in correlation
Octanethiol, by Merck Group (1 mentions)
Toluene, by Daejung Chemicals (1 mentions)
Acetone, by Merck Group (1 mentions)
Potassium hydroxide, by Merck Group (1 mentions)
Styrene, by Merck Group (1 mentions)
Dichloromethane, by Thermo Fisher Scientific (1 mentions)
N hexane, by Avantor (1 mentions)
Acryloyl chloride, by Merck Group (1 mentions)
Carbon disulfide, by Merck Group (1 mentions)
4 4 0 azobis 4 cyanopentanoic acid, by Merck Group (1 mentions)
Pyrrolidine, by Merck Group (1 mentions)
Methyl acetate, by Merck Group (1 mentions)
1 4 dioxane, by Avantor (1 mentions)
2 protocols using butanethiol
1
Surface Modification of Ag/Cu Powders
2
Synthesis and Purification of RAFT Agents
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Styrene (Sigma Aldrich, 99%) was deinhibited over activated basic alumina prior to each polymerization. The RAFT agents TTC 2 (ABCR, 97%) and TTC 3 (ABCR, 97%) were used as received. The chemicals used as reactants, acryloyl chloride (ABCR, 96%, stabilized with phenothiazine), pyrrolidine (Acros, 99%), butanethiol (Sigma Aldrich, 99%), potassium hydroxide (Merck, 485%), carbon disulfide (Merck, 99%), p-tosyl chloride (Merck, 98%), and 4,4 0 -azobis(4-cyanopentanoic acid) (Sigma Aldrich, 98%) were used as received. All solvents for reactions, purifications, and NMR, dichloromethane (Acros, 99.9%), 1,4-dioxane (Gru ¨ssing, 99%), dimethylformamide (VWR, 99.5%), acetone (Merck, 99%), methyl acetate (Merck, 99%), n-hexane (VWR Chemicals, 95%), chloroform-d 1 (Euriso-Top, 99.8%), and tetrahydrofuran-d 8 (Euriso-Top, 99.5%) were used without further purification. All other chemicals, sodium chloride Gru ¨ssing (99%), KHSO 4 (Gru ¨ssing, 99%), NaHCO 3 (Gru ¨ssing, 99%), Mg 2 SO 4 (Gru ¨ssing, 99%), and activated basic aluminum oxide (Merck, 99%, grain size between 0.063-0.200 mm) were also used as received.
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