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2 protocols using iron 2 chloride tetrahydrate

1

Synthesis of Functionalized Silica Nanoparticles

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L-tryptophan (98%), decanoyl chloride (98%), sodium hydroxide (97%), sodium bicarbonate (97%), 3-aminopropyl trimethoxysilane (97%), tetraethyl orthosilicate (98%), butyric acid (99%), cetyltrimethylammonium bromide (99%), and dichloromethane (99.8%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Tetrahydrofuran (TFH, 99.5%), hydrochloric acid (35% w/w), oleic acid (99%), palmitic acid (99%), citric acid (99%), ammonia solution (32% w/w), iron (III) chloride (97%), iron (II) chloride tetrahydrate (99%), and sodium chloride (99.5%) were supplied by Scharlab (Barcelona, Spain).
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2

Synthesis of Carbon Nanotube Composites

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Carbon nanotubes were purchased from Shenzhen Nanotech port Co. Ltd, Shenzhen, China. They are in the form of multiwalled carbon nanotubes CNTs with dimensions of 5–15 μm length and 10–30 nm external diameter. Cobalt (II) chloride hexahydrate (GCC, United Kingdom), Iron (II) chloride tetrahydrate (BDH, England), Iron (III) chloride hexahydrate (Scharlau, Spain), Titanium (IV) isopropoxide (Sigma Aldrich, United States) were used. All chemicals used were analytical grade unless stated otherwise. Triply distilled water was used to prepare all solutions.
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