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2 protocols using lead iodide

1

Synthesis and Characterization of High-Purity Perovskite Materials

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Tin iodide (SnI2, 99.999%) was purchased from Alfa Aesar. DMSO (99.8%), N,N‐dimethylformamide (DMF, 99.8%), tin fluoride (SnF2, 99%), TAH (98%), chlorobenzene (CB anhydrous, 99.8%), and tin powders (<150 µm, 99.5%) were purchased from Sigma–Aldrich. Methylammonium iodide (MAI), FAI, and lead iodide (PbI2) were purchased from GreatCell Solar. Fullerene (C60) and bathocuproine (BCP) were obtained from Xi'an Polymer Light Technology Co. Ltd., China. PEDOT:PSS aqueous solution (Al 4083) was acquired from Heraeus Clevios. All the chemical reagents were used as received without any further purification.
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2

Perovskite Solar Cell Fabrication

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Lead
iodide (PbI2, TCI), lead
bromide (PbBr2, TCI), formamidinium iodide (FAI, Greatcell
Solar Materials), methylammonium bromide (MABr, Greatcell Solar Materials), n-hexyl trimethylammonium bromide (HTABr, Greatcell Solar
Materials), polyethylenoxide (PEO, Sigma-Aldrich), methylammonium
chloride (MACl, Sigma-Aldrich), spiro-OMeTAD (Luminescence Technology
corp.), FK209 (Luminescence Technology corp.), creatine (Sigma-Aldrich),
hydriodic acid (Alfa Aesar), SnO2 colloidal solution (Alfa
Aesar), dimethylformamide (DMF, Sigma-Aldrich), dimethyl sulfoxide
(DMSO, Sigma-Aldrich), isopropyl alcohol (IPA, Sigma-Aldrich), chlorobenzene
(CB, Sigma-Aldrich), diethyl ether (DEE, Sigma-Aldrich), acetone (Sigma-Aldrich),
and ethanol (Sigma-Aldrich)
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