1,2-Ethylenediamine
(99%) was obtained from Sinopharm Chemical Reagent Co., Ltd. (Shanghai,
China). Acrylic acid (99%), glycidyl methacrylate (GMA, 97%), 2,2′-azodiisobutyronitrile
(AIBN, 99%) and methyl methacrylate (MMA, 99%), and all other reagents
purchased from Aladdin Industrial Corporation (Shanghai, China) were
used directly in the as-received condition without further purification.
PMMA (
Mw = 43 982) used in this
work was supplied by Alfa Aesar (Shanghai, China). Photoluminescence
(PL) emission spectra were performed on an RF-5301 PC spectrophotometer
with a 450W xenon lamp as the excitation source. FTIR spectra were
measured on a Nexus 912 AO446 spectrophotometer in the range of 4000–400
cm
–1.
1H NMR spectra of the samples were
measured with an Ascend 400 spectrometer with D
2O and deuterated
chloroform as solvents. The morphology and microstructure of the CQDs
were determined by high-resolution transmission electron microscopy
(HRTEM) on a Philips
Tecnai G2 F30 microscope with an accelerating
voltage of 200 kV. UV–vis absorption spectra were measured
on a UV–vis spectrophotometer Lambda 750. X-ray photoelectric
spectrometry (XPS) was performed on a PHI 5000 VersaProbe to reveal
the interaction between the elements of the CQDs.
Li Y., Wang Y.Q., Liu D., Gao Y., Wang S.N, & Qiu H. (2021). Dual-Emission Ratiometric Fluorescent Probe Based on Lanthanide-Functionalized Carbon Quantum Dots for White Light Emission and Chemical Sensing. ACS Omega, 6(22), 14629-14638.