Optical rotations were measured on a P2010 polarimeter (JASCO Inc, Easton, MD, USA). Low-resolution electrospray ionization (ESI) mass spectra were measured on a 6120 Quadrupole HPLC/MS system (Agilent, Santa Clara, CA, USA) equipped with a Kinetex C18 (2) 5 μm column (4.6 mm × 250 mm, Phenomenex, Torrance, CA, USA). High-resolution ESI-MS data were obtained using an Agilent iFunnel 6550 Q-TOF (quadrupole time-of-flight) MS instrument. NMR spectra including 2D-NMR (gCOSY, gHSQC, and gHMBC) were recorded on an Agilent 600 MHz NMR spectrometer equipped with a cold probe. Chemical shifts were referenced to residual solvents. A Sep-Pak® Vac 35cc (10 g) C18 cartridge (Waters, Milford, MA, USA) was used for flash column chromatography. The separation of crude extracts was performed on an Agilent Prepstar HPLC system using an Agilent Polaris C18-A 5 μm (21.2 mm × 250 mm) column and a Phenomenex Luna C18 or C8 (2) 10 μm column (10.0 mm × 250 mm).
6120 quadrupole hplc ms system
Manufactured by Agilent Technologies
Sourced in United States
The 6120 Quadrupole HPLC/MS system is a liquid chromatography-mass spectrometry (LC/MS) instrument designed for analytical applications. It combines high-performance liquid chromatography (HPLC) with a quadrupole mass spectrometer to enable the separation, identification, and quantification of chemical compounds in complex samples.
Automatically generated - may contain errors
Lab products found in correlation
600 mhz nmr spectrometer, by Agilent Technologies (2 mentions)
6550 ifunnel q tof, by Agilent Technologies (2 mentions)
Luna c18, by Phenomenex (2 mentions)
Kinetex c18 2 5 μm column, by Phenomenex (2 mentions)
Sep pak vac 35cc 10g c18 cartridge, by Waters Corporation (2 mentions)
Prepstar hplc system, by Agilent Technologies (2 mentions)
Polaris c18 a 5 μm, by Phenomenex (2 mentions)
P2010 polarimeter, by Jasco (2 mentions)
C8 2 10 μm column, by Phenomenex (2 mentions)
2 protocols using 6120 quadrupole hplc ms system
1
Analytical Techniques for Natural Product Characterization
2
Analytical Techniques for Natural Product Characterization
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Optical rotations were measured on a P2010 polarimeter (JASCO Inc, Easton, MD, USA). Low-resolution electrospray ionization (ESI) mass spectra were measured on a 6120 Quadrupole HPLC/MS system (Agilent, Santa Clara, CA, USA) equipped with a Kinetex C18 (2) 5 μm column (4.6 mm × 250 mm, Phenomenex, Torrance, CA, USA). High-resolution ESI-MS data were obtained using an Agilent iFunnel 6550 Q-TOF (quadrupole time-of-flight) MS instrument. NMR spectra including 2D-NMR (gCOSY, gHSQC, and gHMBC) were recorded on an Agilent 600 MHz NMR spectrometer equipped with a cold probe. Chemical shifts were referenced to residual solvents. A Sep-Pak® Vac 35cc (10 g) C18 cartridge (Waters, Milford, MA, USA) was used for flash column chromatography. The separation of crude extracts was performed on an Agilent Prepstar HPLC system using an Agilent Polaris C18-A 5 μm (21.2 mm × 250 mm) column and a Phenomenex Luna C18 or C8 (2) 10 μm column (10.0 mm × 250 mm).
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